benzyl [(2S)-2-[(tert-butoxycarbonyl)amino]-3-(dimethylamino)-3-oxopropyl]carbamate

Base Information

Chemical Name:benzyl [(2S)-2-[(tert-butoxycarbonyl)amino]-3-(dimethylamino)-3-oxopropyl]carbamate
CAS No.:721927-40-8
Molecular Formula:C₁₈H₂₇N₃O₅
Molecular Weight:365.429
Hs Code.:

Synonyms:benzyl [(2S)-2-[(tert-butoxycarbonyl)amino]-3-(dimethylamino)-3-oxopropyl]carbamate

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Chemical Property of benzyl [(2S)-2-[(tert-butoxycarbonyl)amino]-3-(dimethylamino)-3-oxopropyl]carbamate

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Technology Process of benzyl [(2S)-2-[(tert-butoxycarbonyl)amino]-3-(dimethylamino)-3-oxopropyl]carbamate

There total 3 articles about benzyl [(2S)-2-[(tert-butoxycarbonyl)amino]-3-(dimethylamino)-3-oxopropyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 506-59-2
N,N-dimethylammonium chloride

: 65710-57-8,81306-93-6
3-{[(benzyloxy)carbonyl]amino}-N-(tert-butoxycarbonyl)-L-alanine

: 721927-40-8
benzyl [(2S)-2-[(tert-butoxycarbonyl)amino]-3-(dimethylamino)-3-oxopropyl]carbamate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield:

: 506-59-2
N,N-dimethylammonium chloride

: 76387-70-7
(S)-3-amino-2-tert-butoxycarbonylaminopropionic acid

: 501-53-1,94274-21-2
benzyl chloroformate

: 721927-40-8
benzyl [(2S)-2-[(tert-butoxycarbonyl)amino]-3-(dimethylamino)-3-oxopropyl]carbamate

Guidance literature:: (S)-3-amino-2-tert-butoxycarbonylaminopropionic acid; benzyl chloroformate; With sodium hydrogencarbonate; In water; acetone; at 20 ℃; for 1.5h;

N,N-dimethylammonium chloride; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In DMF (N,N-dimethyl-formamide); at 20 ℃;

Reference yield:

: 65710-57-8,81306-93-6
3-{[(benzyloxy)carbonyl]amino}-N-(tert-butoxycarbonyl)-L-alanine

: 124-40-3
dimethyl amine

: 721927-40-8
benzyl [(2S)-2-[(tert-butoxycarbonyl)amino]-3-(dimethylamino)-3-oxopropyl]carbamate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2007.07.028