C₁₅H₁₄FN

Base Information

• Chemical Name: C₁₅H₁₄FN
• CAS No.: 1253935-32-8
• Molecular Formula: C₁₅H₁₄FN
• Molecular Weight: 227.281
• Mol file: 1253935-32-8.mol

Synonyms:C₁₅H₁₄FN

Chemical Property of C₁₅H₁₄FN

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₁₅H₁₄FN

There total 2 articles about C₁₅H₁₄FN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

C15H14FN3 (1253935-25-9) → C15H14FN (1253935-32-8)

Guidance literature:

With 5,10,15,20-tetrakis(pentafluorophenyl)-21H,23H-porphyrin iron(III) chloride; In 1,2-dichloro-ethane; for 14h; Molecular sieve; Reflux; Inert atmosphere;

DOI:10.1039/c0cc01825b

Reference yield: 69.0%

5-fluoro-2-nitrobenzaldehyde (395-81-3) + acetophenone (98-86-2) → C15H14FN (1253935-32-8)

Guidance literature:

5-fluoro-2-nitrobenzaldehyde; acetophenone; In toluene; at 80 ℃; for 5h;

With hydrogen; In toluene; at 80 ℃; for 19h; under 5175.52 Torr;

DOI:10.1039/d1cy00418b

upstream raw materials:

C₁₅H₁₄FN₃

5-fluoro-2-nitrobenzaldehyde

acetophenone

Refernces

• 1、 Liu, Yungen,Wei, Jinhu,Che, Chi-Ming. "[Fe(F20TPP)Cl] catalyzed intramolecular C-N bond formation for alkaloid synthesis using aryl azides as nitrogen source". supporting information; experimental part. p. 6926 - 6928. Retrieved 2010/11/16.