4-(3-chloro-4-isopropoxyphenylamino)-1-benzyl-5-(ethoxycarbonyl)pyridine-2(1H)-one

Base Information

Chemical Name:4-(3-chloro-4-isopropoxyphenylamino)-1-benzyl-5-(ethoxycarbonyl)pyridine-2(1H)-one
CAS No.:1359815-29-4
Molecular Formula:C₂₄H₂₅ClN₂O₄
Molecular Weight:440.927
Hs Code.:

Synonyms:4-(3-chloro-4-isopropoxyphenylamino)-1-benzyl-5-(ethoxycarbonyl)pyridine-2(1H)-one

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Chemical Property of 4-(3-chloro-4-isopropoxyphenylamino)-1-benzyl-5-(ethoxycarbonyl)pyridine-2(1H)-one

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Technology Process of 4-(3-chloro-4-isopropoxyphenylamino)-1-benzyl-5-(ethoxycarbonyl)pyridine-2(1H)-one

There total 4 articles about 4-(3-chloro-4-isopropoxyphenylamino)-1-benzyl-5-(ethoxycarbonyl)pyridine-2(1H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1359818-45-3
4-chloro-1-benzyl-5-(ethoxycarbonyl-)pyridine-2(1H)-one

: 5211-04-1
3-Chloro-4-isopropoxy-phenylamine

: 1359815-29-4
4-(3-chloro-4-isopropoxyphenylamino)-1-benzyl-5-(ethoxycarbonyl)pyridine-2(1H)-one

Guidance literature:: With palladium diacetate; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,4-dioxane; for 1h; Reflux;

Reference yield:

: 100-46-9
benzylamine

: 1359815-29-4
4-(3-chloro-4-isopropoxyphenylamino)-1-benzyl-5-(ethoxycarbonyl)pyridine-2(1H)-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: orthoformic acid triethyl ester; acetic anhydride / 15 h / Reflux

1.2: 2.33 h / 20 - 90 °C

2.1: trichlorophosphate / 1 h / 90 °C

3.1: 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; palladium diacetate; caesium carbonate / 1,4-dioxane / 1 h / Reflux

With palladium diacetate; acetic anhydride; caesium carbonate; orthoformic acid triethyl ester; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; trichlorophosphate; In 1,4-dioxane;

Reference yield:

: 343348-34-5
1-benzyl-5-ethoxycarbonyl-4-hydroxypyridine-2(1H)-one

: 1359815-29-4
4-(3-chloro-4-isopropoxyphenylamino)-1-benzyl-5-(ethoxycarbonyl)pyridine-2(1H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: trichlorophosphate / 1 h / 90 °C

2: 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; palladium diacetate; caesium carbonate / 1,4-dioxane / 1 h / Reflux

With palladium diacetate; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; trichlorophosphate; In 1,4-dioxane;