3-(4,4,6-trimethyl-1,3,2-dioxaborato)-6-phenylhexanoic acid N,N-methoxymethylamide

Base Information

Chemical Name:3-(4,4,6-trimethyl-1,3,2-dioxaborato)-6-phenylhexanoic acid N,N-methoxymethylamide
CAS No.:1316253-52-7
Molecular Formula:C₂₀H₃₂BNO₄
Molecular Weight:361.289
Hs Code.:

Synonyms:3-(4,4,6-trimethyl-1,3,2-dioxaborato)-6-phenylhexanoic acid N,N-methoxymethylamide

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Chemical Property of 3-(4,4,6-trimethyl-1,3,2-dioxaborato)-6-phenylhexanoic acid N,N-methoxymethylamide

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Technology Process of 3-(4,4,6-trimethyl-1,3,2-dioxaborato)-6-phenylhexanoic acid N,N-methoxymethylamide

There total 3 articles about 3-(4,4,6-trimethyl-1,3,2-dioxaborato)-6-phenylhexanoic acid N,N-methoxymethylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 10199-14-1,23894-82-8
4,4,6-trimethyl-1,3,2-dioxaborinane

: 1316253-39-0
(E)-6-phenyl-3-hexenoic acid N,O-dimethylhydroxylamide

: 1316253-52-7
3-(4,4,6-trimethyl-1,3,2-dioxaborato)-6-phenylhexanoic acid N,N-methoxymethylamide

Guidance literature:: With bis(norbornadiene)rhodium(l)tetrafluoroborate; (R)-(+)-1,1'-bi-2-naphthol; In tetrahydrofuran; at 0 - 40 ℃; Inert atmosphere;
DOI:10.1039/c1cc11746g

Reference yield:

: 107-41-5
2-methyl-2,4-pentanediol

: 1316253-52-7
3-(4,4,6-trimethyl-1,3,2-dioxaborato)-6-phenylhexanoic acid N,N-methoxymethylamide

Guidance literature:: Multi-step reaction with 2 steps

1: borane dimethyl sulphide complex / dichloromethane / 2 h / 0 °C / Inert atmosphere

2: (R)-(+)-1,1'-bi-2-naphthol; bis(norbornadiene)rhodium(l)tetrafluoroborate / tetrahydrofuran / 0 - 40 °C / Inert atmosphere

With bis(norbornadiene)rhodium(l)tetrafluoroborate; borane dimethyl sulphide complex; (R)-(+)-1,1'-bi-2-naphthol; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c1cc11746g

Reference yield:

: 1016225-28-7
(E)-6-phenyl-3-hexenoic acid

: 1316253-52-7
3-(4,4,6-trimethyl-1,3,2-dioxaborato)-6-phenylhexanoic acid N,N-methoxymethylamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1,1'-carbonyldiimidazole / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

1.2: 5 h / 0 - 20 °C / Inert atmosphere

2.1: (R)-(+)-1,1'-bi-2-naphthol; bis(norbornadiene)rhodium(l)tetrafluoroborate / tetrahydrofuran / 0 - 40 °C / Inert atmosphere

With bis(norbornadiene)rhodium(l)tetrafluoroborate; (R)-(+)-1,1'-bi-2-naphthol; 1,1'-carbonyldiimidazole; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c1cc11746g