(S)-8-methyl-6-phenyl-2,3,4,7,8,10-hexahydro-1H-pyrano[4,3-c][1,6]naphthyridine

Base Information

• Chemical Name: (S)-8-methyl-6-phenyl-2,3,4,7,8,10-hexahydro-1H-pyrano[4,3-c][1,6]naphthyridine
• CAS No.: 1036733-28-4
• Molecular Formula: C₁₈H₂₀N₂O
• Molecular Weight: 280.37

Synonyms:(S)-8-methyl-6-phenyl-2,3,4,7,8,10-hexahydro-1H-pyrano[4,3-c][1,6]naphthyridine

Chemical Property of (S)-8-methyl-6-phenyl-2,3,4,7,8,10-hexahydro-1H-pyrano[4,3-c][1,6]naphthyridine

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Technology Process of (S)-8-methyl-6-phenyl-2,3,4,7,8,10-hexahydro-1H-pyrano[4,3-c][1,6]naphthyridine

There total 1 articles about (S)-8-methyl-6-phenyl-2,3,4,7,8,10-hexahydro-1H-pyrano[4,3-c][1,6]naphthyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

(S)-2-(4-methoxybenzyl)-8-methyl-6-phenyl-2,3,4,7,8,10-hexahydro-1H-pyrano[4,3-c][1,6]naphthyridine (1036733-24-0) → (S)-8-methyl-6-phenyl-2,3,4,7,8,10-hexahydro-1H-pyrano[4,3-c][1,6]naphthyridine (1036733-28-4)

Guidance literature:

With hydrogen; acetic acid; palladium on carbon; In methanol; water; at 20 ℃; for 12h;

Reference yield: 85.0%

Methoxyacetyl chloride (38870-89-2) + (S)-8-methyl-6-phenyl-2,3,4,7,8,10-hexahydro-1H-pyrano[4,3-c][1,6]naphthyridine (1036733-28-4) → (S)-2-Methoxy-1-(8-methyl-6-phenyl-3,4,7,8-tetrahydro-1H-pyrano[4,3-c][1,6]naphthyridin-2(10H)-yl)ethanone (958753-92-9)

Guidance literature:

With PS-DMAP; In dichloromethane; at 20 ℃; for 10h;

Reference yield: 82.0%

(S)-8-methyl-6-phenyl-2,3,4,7,8,10-hexahydro-1H-pyrano[4,3-c][1,6]naphthyridine (1036733-28-4) + isobutyraldehyde (78-84-2) → C22H28N2O

Guidance literature:

With sodium cyanoborohydride; acetic acid; In methanol; at 20 ℃; for 12h;

upstream raw materials:

(S)-2-(4-methoxybenzyl)-8-methyl-6-phenyl-2,3,4,7,8,10-hexahydro-1H-pyrano[4,3-c][1,6]naphthyridine

Downstream raw materials:

(S)-2-Methoxy-1-(8-methyl-6-phenyl-3,4,7,8-tetrahydro-1H-pyrano[4,3-c][1,6]naphthyridin-2(10H)-yl)ethanone

C₂₅H₂₆N₂O₃S

C₂₇H₂₉N₃O₂

(S)-methyl 3-methyl-2-((S)-8-methyl-6-phenyl-2,3,4,7,8,10-hexahydro-1H-pyrano[4,3-c][1,6]naphthyridine-2-carboxamido)butanoate

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