C₃₄H₃₉N₃O₈

Base Information

Chemical Name:C₃₄H₃₉N₃O₈
CAS No.:1338925-52-2
Molecular Formula:C₃₄H₃₉N₃O₈
Molecular Weight:617.699
Hs Code.:

C<sub>34</sub>H<sub>39</sub>N<sub>3</sub>O<sub>8</sub>

Synonyms:C₃₄H₃₉N₃O₈

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Chemical Property of C₃₄H₃₉N₃O₈

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Technology Process of C₃₄H₃₉N₃O₈

There total 13 articles about C₃₄H₃₉N₃O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1338925-51-1
C₄₀H₅₁BIN₃O₁₀

: 1338925-52-2
C₃₄H₃₉N₃O₈

Guidance literature:: With bis(tri-t-butylphosphine)palladium⁽⁰⁾; potassium carbonate; In dimethyl sulfoxide; at 90 ℃; for 24h; Inert atmosphere;
DOI:10.1021/ja207318n

Reference yield:

: 1086703-03-8
(S)-2-(tert-butoxycarbonyl(methyl)amino)-2-(4-hydroxy-3-iodophenyl)acetic acid

: 1338925-52-2
C₃₄H₃₉N₃O₈

Guidance literature:: Multi-step reaction with 6 steps

1: triethylsilane; trifluoroacetic acid / 24 h / 0 - 20 °C

2: sodium hydrogencarbonate; sodium hydroxide / tetrahydrofuran; water / 8 h / 0 - 20 °C / pH 7

3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 0 - 20 °C

4: trimethyltin(IV) hydroxide / 1,2-dichloro-ethane / 4 h / 20 - 75 °C / Inert atmosphere

5: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide; acetonitrile / 0 - 20 °C

6: bis(tri-t-butylphosphine)palladium⁽⁰⁾; potassium carbonate / dimethyl sulfoxide / 24 h / 90 °C / Inert atmosphere

With triethylsilane; bis(tri-t-butylphosphine)palladium⁽⁰⁾; sodium hydrogencarbonate; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trimethyltin(IV) hydroxide; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; water; dimethyl sulfoxide; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ja207318n

Reference yield:

: C₉H₁₀INO₃

: 1338925-52-2
C₃₄H₃₉N₃O₈

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydrogencarbonate; sodium hydroxide / tetrahydrofuran; water / 8 h / 0 - 20 °C / pH 7

2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 0 - 20 °C

3: trimethyltin(IV) hydroxide / 1,2-dichloro-ethane / 4 h / 20 - 75 °C / Inert atmosphere

4: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide; acetonitrile / 0 - 20 °C

5: bis(tri-t-butylphosphine)palladium⁽⁰⁾; potassium carbonate / dimethyl sulfoxide / 24 h / 90 °C / Inert atmosphere

With bis(tri-t-butylphosphine)palladium⁽⁰⁾; sodium hydrogencarbonate; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trimethyltin(IV) hydroxide; sodium hydroxide; In tetrahydrofuran; water; dimethyl sulfoxide; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ja207318n