C₁₆H₂₄FNO₂S

Base Information

Chemical Name:C₁₆H₂₄FNO₂S
CAS No.:1309653-57-3
Molecular Formula:C₁₆H₂₄FNO₂S
Molecular Weight:313.436
Hs Code.:

C<sub>16</sub>H<sub>24</sub>FNO<sub>2</sub>S

Synonyms:C₁₆H₂₄FNO₂S

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Chemical Property of C₁₆H₂₄FNO₂S

Chemical Property:

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Technology Process of C₁₆H₂₄FNO₂S

There total 6 articles about C₁₆H₂₄FNO₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1309653-56-2
C₁₅H₂₀FNO₂S

: 75-16-1
methylmagnesium bromide

: 1309653-57-3
C₁₆H₂₄FNO₂S

Guidance literature:: C₁₅H₂₀FNO₂S; methylmagnesium bromide; In tetrahydrofuran; diethyl ether; at 0 - 20 ℃; for 2h;

With ammonium chloride; In tetrahydrofuran; diethyl ether; water; at 0 ℃; for 0.166667h;

Reference yield:

: 51446-31-2
4-fluoro-3-hydroxybenzoic acid

: 1309653-57-3
C₁₆H₂₄FNO₂S

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 6 h / 90 °C

1.2: 2 h / 0 °C

2.1: manganese(IV) oxide / dichloromethane / 6 h / 45 °C

3.1: titanium(IV) isopropylate / toluene / 6 h / 75 °C

4.1: tetrahydrofuran; diethyl ether / 2 h / 0 - 20 °C

4.2: 0.17 h / 0 °C

With titanium(IV) isopropylate; manganese(IV) oxide; potassium carbonate; potassium iodide; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide; toluene;

Reference yield:

: 351317-28-7
ethyl 3-hydroxy-4-fluorobenzoate

: 1309653-57-3
C₁₆H₂₄FNO₂S

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 3.5 h / 90 °C

2.1: lithium borohydride / tetrahydrofuran / 3.5 h / 80 °C

2.2: 0 °C

3.1: manganese(IV) oxide / dichloromethane / 6 h / 45 °C

4.1: titanium(IV) isopropylate / toluene / 6 h / 75 °C

5.1: tetrahydrofuran; diethyl ether / 2 h / 0 - 20 °C

5.2: 0.17 h / 0 °C

With titanium(IV) isopropylate; manganese(IV) oxide; lithium borohydride; potassium carbonate; potassium iodide; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide; toluene;