t-butyl 3-(benzyloxycarbonyl)benzyl-3-ethoxycarbonylacetyl-2-methylcarbazate

Base Information

Chemical Name:t-butyl 3-(benzyloxycarbonyl)benzyl-3-ethoxycarbonylacetyl-2-methylcarbazate
CAS No.:111709-20-7
Molecular Formula:C₂₆H₃₂N₂O₇
Molecular Weight:484.549
Hs Code.:

Synonyms:t-butyl 3-(benzyloxycarbonyl)benzyl-3-ethoxycarbonylacetyl-2-methylcarbazate

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Chemical Property of t-butyl 3-(benzyloxycarbonyl)benzyl-3-ethoxycarbonylacetyl-2-methylcarbazate

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Technology Process of t-butyl 3-(benzyloxycarbonyl)benzyl-3-ethoxycarbonylacetyl-2-methylcarbazate

There total 5 articles about t-butyl 3-(benzyloxycarbonyl)benzyl-3-ethoxycarbonylacetyl-2-methylcarbazate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 111709-19-4
t-butyl 3-(benzyloxycarbonyl)benzyl-2-methylcarbazate

: 36239-09-5
ethyl chlorocarbonylacetate

: 111709-20-7
t-butyl 3-(benzyloxycarbonyl)benzyl-3-ethoxycarbonylacetyl-2-methylcarbazate

Guidance literature:: With triethylamine; In benzene; for 12h; Ambient temperature;

Reference yield:

: 870-46-2
t-butoxycarbonylhydrazine

: 111709-20-7
t-butyl 3-(benzyloxycarbonyl)benzyl-3-ethoxycarbonylacetyl-2-methylcarbazate

Guidance literature:: Multi-step reaction with 4 steps

1: 81 percent / acetic acid / ethanol / 3 h / Heating

2: 95 percent / K₂CO₃ / acetone / 24 h / Heating

3: 57 percent / NaBH₃CN, aq. HCl / tetrahydrofuran; methanol

4: 50 percent / triethylamine / benzene / 12 h / Ambient temperature

With hydrogenchloride; sodium cyanoborohydride; potassium carbonate; acetic acid; triethylamine; In tetrahydrofuran; methanol; ethanol; acetone; benzene;

Reference yield:

: 62977-82-6
benzyl oxo(phenyl)acetate

: 111709-20-7
t-butyl 3-(benzyloxycarbonyl)benzyl-3-ethoxycarbonylacetyl-2-methylcarbazate

Guidance literature:: Multi-step reaction with 4 steps

1: 81 percent / acetic acid / ethanol / 3 h / Heating

2: 95 percent / K₂CO₃ / acetone / 24 h / Heating

3: 57 percent / NaBH₃CN, aq. HCl / tetrahydrofuran; methanol

4: 50 percent / triethylamine / benzene / 12 h / Ambient temperature

With hydrogenchloride; sodium cyanoborohydride; potassium carbonate; acetic acid; triethylamine; In tetrahydrofuran; methanol; ethanol; acetone; benzene;