3-(2-benzyloxy-3,5-dibromo-4-methoxyphenyl)-2-benzyloxyiminopropanoic acid

Base Information

Chemical Name:3-(2-benzyloxy-3,5-dibromo-4-methoxyphenyl)-2-benzyloxyiminopropanoic acid
CAS No.:35031-38-0
Molecular Formula:C₂₄H₂₁Br₂NO₅
Molecular Weight:563.242
Hs Code.:

Synonyms:3-(2-benzyloxy-3,5-dibromo-4-methoxyphenyl)-2-benzyloxyiminopropanoic acid

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Chemical Property of 3-(2-benzyloxy-3,5-dibromo-4-methoxyphenyl)-2-benzyloxyiminopropanoic acid

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Technology Process of 3-(2-benzyloxy-3,5-dibromo-4-methoxyphenyl)-2-benzyloxyiminopropanoic acid

There total 4 articles about 3-(2-benzyloxy-3,5-dibromo-4-methoxyphenyl)-2-benzyloxyiminopropanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 2687-43-6
O-benzylhydoxylamine hydrochloride

: (Z)-4-(2-(benzyloxy)-3,5-dibromo-4-methoxybenzylidene)-2-methyloxazol-5(4H)-one

: 35031-38-0
3-(2-benzyloxy-3,5-dibromo-4-methoxyphenyl)-2-benzyloxyiminopropanoic acid

Guidance literature:: (Z)-4-(2-(benzyloxy)-3,5-dibromo-4-methoxybenzylidene)-2-methyloxazol-5(4H)-one; With barium dihydroxide; In 1,4-dioxane; at 60 ℃; for 1h;

O-benzylhydoxylamine hydrochloride; In 1,4-dioxane; at 60 ℃; for 14h;
DOI:10.1021/jm051030l

Reference yield:

: 35031-47-1
2-(benzyloxy)-3,5-dibromo-4-methoxybenzaldehyde

: 35031-38-0
2-[(benzyloxy)imino]-3-[2-(benzyloxy)-3,5-dibromo-4-methoxyphenyl]-propanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: (i) NaOAc, Ac₂O, (ii) acetone, H₂O

2: aq. HCl / tetrahydrofuran

With hydrogenchloride; In tetrahydrofuran;
DOI:10.1039/P19720000018

Reference yield:

: 35031-39-1
(E)-2-Acetylamino-3-(2-benzyloxy-3,5-dibromo-4-methoxy-phenyl)-acrylic acid

: 35031-38-0
2-[(benzyloxy)imino]-3-[2-(benzyloxy)-3,5-dibromo-4-methoxyphenyl]-propanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: aq. HCl / tetrahydrofuran

With hydrogenchloride; In tetrahydrofuran;
DOI:10.1039/P19720000018