[1,1'-biphenyl]-2,2'-diylbis(bis(3,5-di-tert-butyl-4-methoxyphenyl)phosphine oxide)

Base Information

Chemical Name:[1,1'-biphenyl]-2,2'-diylbis(bis(3,5-di-tert-butyl-4-methoxyphenyl)phosphine oxide)
CAS No.:1026682-39-2
Molecular Formula:C₇₂H₁₀₀O₆P₂
Molecular Weight:1123.53
Hs Code.:

Synonyms:[1,1'-biphenyl]-2,2'-diylbis(bis(3,5-di-tert-butyl-4-methoxyphenyl)phosphine oxide)

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Chemical Property of [1,1'-biphenyl]-2,2'-diylbis(bis(3,5-di-tert-butyl-4-methoxyphenyl)phosphine oxide)

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Technology Process of [1,1'-biphenyl]-2,2'-diylbis(bis(3,5-di-tert-butyl-4-methoxyphenyl)phosphine oxide)

There total 5 articles about [1,1'-biphenyl]-2,2'-diylbis(bis(3,5-di-tert-butyl-4-methoxyphenyl)phosphine oxide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 17763-95-0
2,2'-bis-<<(trifluoromethyl)sulfonyl>oxy>biphenyl

: 535925-40-7
bis(3,5-di-tert-butyl-4-methoxy-phenyl)phosphine oxide

: 1026682-39-2
[1,1'-biphenyl]-2,2'-diylbis(bis(3,5-di-tert-butyl-4-methoxyphenyl)phosphine oxide)

Guidance literature:: With 1,4-di(diphenylphosphino)-butane; palladium diacetate; In dimethyl sulfoxide; at 100 ℃;
DOI:10.1021/ol0068896

Reference yield: 50.0%

: C₃₆H₅₀IO₂P

: 1026682-39-2
[1,1'-biphenyl]-2,2'-diylbis(bis(3,5-di-tert-butyl-4-methoxyphenyl)phosphine oxide)

Guidance literature:: With copper; In N,N-dimethyl-formamide; at 140 ℃; for 2h;
DOI:10.1021/acs.joc.9b01933

Reference yield: 41.0%

: 1516-96-7
4-bromo-2,6-di-tert-butylanisole

: [1,1'-biphenyl]-2,2'-diylbis(phosphonic dichloride)

: 1026682-39-2
[1,1'-biphenyl]-2,2'-diylbis(bis(3,5-di-tert-butyl-4-methoxyphenyl)phosphine oxide)

Guidance literature:: 4-bromo-2,6-di-tert-butylanisole; With magnesium; In tetrahydrofuran; ethylene dibromide;

[1,1'-biphenyl]-2,2'-diylbis(phosphonic dichloride); In tetrahydrofuran; ethylene dibromide; at -78 - 20 ℃; for 12h;
DOI:10.1021/acs.orglett.9b02439