Technology Process of C16H15F3O4S
There total 2 articles about C16H15F3O4S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: N-benzyl-N,N,N-triethylammonium chloride; palladium diacetate; sodium hydrogencarbonate / N,N-dimethyl-formamide / 20 h / 45 °C / Inert atmosphere
2.1: L-proline / water; dimethyl sulfoxide / 0.5 h / 30 °C
3.1: methanol; sodium tetrahydroborate / water; dimethyl sulfoxide / 0.5 h / 0 °C
4.1: palladium 10% on activated carbon; chloroform; hydrogen / ethanol / 12 h
5.1: triethylamine / dichloromethane / 0 °C / Inert atmosphere
5.2: 15 h / 20 °C / Inert atmosphere
With
methanol; sodium tetrahydroborate; chloroform; palladium 10% on activated carbon; N-benzyl-N,N,N-triethylammonium chloride; hydrogen; palladium diacetate; sodium hydrogencarbonate; triethylamine; L-proline;
In
ethanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
1.1: Heck reaction;
DOI:10.1016/j.tet.2012.01.095
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: methanol; sodium tetrahydroborate / water; dimethyl sulfoxide / 0.5 h / 0 °C
2.1: palladium 10% on activated carbon; chloroform; hydrogen / ethanol / 12 h
3.1: triethylamine / dichloromethane / 0 °C / Inert atmosphere
3.2: 15 h / 20 °C / Inert atmosphere
With
methanol; sodium tetrahydroborate; chloroform; palladium 10% on activated carbon; hydrogen; triethylamine;
In
ethanol; dichloromethane; water; dimethyl sulfoxide;
DOI:10.1016/j.tet.2012.01.095
