C₂₃H₂₅ClF₂O₄S

Base Information

Chemical Name:C₂₃H₂₅ClF₂O₄S
CAS No.:471905-47-2
Molecular Formula:C₂₃H₂₅ClF₂O₄S
Molecular Weight:470.965
Hs Code.:

C<sub>23</sub>H<sub>25</sub>ClF<sub>2</sub>O<sub>4</sub>S

Synonyms:C₂₃H₂₅ClF₂O₄S

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Chemical Property of C₂₃H₂₅ClF₂O₄S

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Technology Process of C₂₃H₂₅ClF₂O₄S

There total 8 articles about C₂₃H₂₅ClF₂O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 74-88-4
methyl iodide

: 471905-47-2
C₂₃H₂₅ClF₂O₄S

Guidance literature:: [4-(4-chloro-benzenesulfonyl)-4-(2,5-difluoro-phenyl)-cyclohexyl]-acetic acid ethyl ester; With sodium hexamethyldisilazane; In tetrahydrofuran; at -78 - 20 ℃; for 2h;

methyl iodide; In tetrahydrofuran; at -20 - 20 ℃; for 2h;

Reference yield:

: 470716-51-9
2-[[(4-chlorophenyl)sulfonyl]methyl]-1,4-difluorobenzene

: 471905-47-2
C₂₃H₂₅ClF₂O₄S

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium tert-butylate / tetrahydrofuran / 2 h

2.1: water; sodium chloride / dimethyl sulfoxide / 2 h / 150 °C

3.1: sodium hydride / tetrahydrofuran / 19.33 h / 20 °C

4.1: sodium tetrahydroborate / nickel dichloride / ethanol / 0.33 h / 20 °C

5.1: sodium hexamethyldisilazane / tetrahydrofuran / 2 h / -78 - 20 °C

5.2: 2 h / -20 - 20 °C

With sodium tetrahydroborate; potassium tert-butylate; water; sodium hexamethyldisilazane; sodium hydride; sodium chloride; nickel dichloride; In tetrahydrofuran; ethanol; dimethyl sulfoxide;

Reference yield:

: 470716-52-0
2-[[(4-chlorophenyl)thio]methyl]-1,4-difluorobenzene

: 471905-47-2
C₂₃H₂₅ClF₂O₄S

Guidance literature:: Multi-step reaction with 6 steps

1.1: m-chloroperoxybenzoic acid / dichloromethane / 2 h

2.1: potassium tert-butylate / tetrahydrofuran / 2 h

3.1: water; sodium chloride / dimethyl sulfoxide / 2 h / 150 °C

4.1: sodium hydride / tetrahydrofuran / 19.33 h / 20 °C

5.1: sodium tetrahydroborate / nickel dichloride / ethanol / 0.33 h / 20 °C

6.1: sodium hexamethyldisilazane / tetrahydrofuran / 2 h / -78 - 20 °C

6.2: 2 h / -20 - 20 °C

With sodium tetrahydroborate; m-chloroperoxybenzoic acid; potassium tert-butylate; water; sodium hexamethyldisilazane; sodium hydride; sodium chloride; nickel dichloride; In tetrahydrofuran; ethanol; dichloromethane; dimethyl sulfoxide;