{4-[1-(4-methylphenyl)-1H-pyrazolo[3,4-c]pyridin-3-yl]morpholin-2-yl}methyl acetate

Base Information

Chemical Name:{4-[1-(4-methylphenyl)-1H-pyrazolo[3,4-c]pyridin-3-yl]morpholin-2-yl}methyl acetate
CAS No.:1427555-84-7
Molecular Formula:C₂₀H₂₂N₄O₃
Molecular Weight:366.42
Hs Code.:

Synonyms:{4-[1-(4-methylphenyl)-1H-pyrazolo[3,4-c]pyridin-3-yl]morpholin-2-yl}methyl acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of {4-[1-(4-methylphenyl)-1H-pyrazolo[3,4-c]pyridin-3-yl]morpholin-2-yl}methyl acetate

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Technology Process of {4-[1-(4-methylphenyl)-1H-pyrazolo[3,4-c]pyridin-3-yl]morpholin-2-yl}methyl acetate

There total 6 articles about {4-[1-(4-methylphenyl)-1H-pyrazolo[3,4-c]pyridin-3-yl]morpholin-2-yl}methyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 5.0%

: 624-31-7
4-tolyl iodide

: 1427555-79-0
(4-{1H-pyrazolo[3,4-c]pyridin-3-yl}morpholin-2-yl)methyl acetate

: 1427555-84-7
{4-[1-(4-methylphenyl)-1H-pyrazolo[3,4-c]pyridin-3-yl]morpholin-2-yl}methyl acetate

Guidance literature:: With potassium phosphate; copper(l) iodide; N,N`-dimethylethylenediamine; In N,N-dimethyl-formamide; at 140 ℃; for 1h; Microwave irradiation;

Reference yield:

: 1427588-82-6
tert-butyl 2-[(acetyloxy)methyl]morpholine-4-carboxylate

: 1427555-84-7
{4-[1-(4-methylphenyl)-1H-pyrazolo[3,4-c]pyridin-3-yl]morpholin-2-yl}methyl acetate

Guidance literature:: Multi-step reaction with 4 steps

1.1: trifluoroacetic acid / dichloromethane

2.1: triethylamine / methanol; 1,2-dichloro-ethane / 0.5 h / 0 °C

2.2: 78 h / 60 °C

3.1: sodium nitrite; acetic acid / water / 0.08 h

4.1: N,N`-dimethylethylenediamine; potassium phosphate; copper(l) iodide / N,N-dimethyl-formamide / 1 h / 140 °C / Microwave irradiation

With potassium phosphate; copper(l) iodide; acetic acid; triethylamine; trifluoroacetic acid; N,N`-dimethylethylenediamine; sodium nitrite; In methanol; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;

Reference yield:

: 1427555-72-3
{4-[(3-aminopyridin-4-yl)methyl]morpholin-2-yl}methyl acetate

: 1427555-84-7
{4-[1-(4-methylphenyl)-1H-pyrazolo[3,4-c]pyridin-3-yl]morpholin-2-yl}methyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium nitrite; acetic acid / water / 0.08 h

2: N,N`-dimethylethylenediamine; potassium phosphate; copper(l) iodide / N,N-dimethyl-formamide / 1 h / 140 °C / Microwave irradiation

With potassium phosphate; copper(l) iodide; acetic acid; N,N`-dimethylethylenediamine; sodium nitrite; In water; N,N-dimethyl-formamide;