methyl 2-amino-5-butylbenzoate

Base Information

Chemical Name:methyl 2-amino-5-butylbenzoate
CAS No.:1183950-19-7
Molecular Formula:C₁₂H₁₇NO₂
Molecular Weight:207.272
Hs Code.:

Synonyms:methyl 2-amino-5-butylbenzoate

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Chemical Property of methyl 2-amino-5-butylbenzoate

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Technology Process of methyl 2-amino-5-butylbenzoate

There total 5 articles about methyl 2-amino-5-butylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67-56-1
methanol

: 18331-73-2
2-amino-5-butylbenzoic acid

: 1183950-19-7
methyl 2-amino-5-butylbenzoate

Guidance literature:: methanol; 2-amino-5-butylbenzoic acid; With thionyl chloride; at 0 - 90 ℃; for 3h; Inert atmosphere;

With sodium hydrogencarbonate; In water;

Reference yield:

: 3663-20-5
N-(4-butylphenyl)acetamide

: 1183950-19-7
methyl 2-amino-5-butylbenzoate

Guidance literature:: Multi-step reaction with 4 steps

1: bromine; acetic acid / 3 h / 0 - 80 °C / Inert atmosphere

2: 1-methyl-pyrrolidin-2-one / 3 h / 140 °C / Inert atmosphere

3: water; sulfuric acid; acetic acid / 3 h / 90 °C / Inert atmosphere

4: thionyl chloride / 3 h / 0 - 90 °C / Inert atmosphere

With thionyl chloride; sulfuric acid; water; bromine; acetic acid; In 1-methyl-pyrrolidin-2-one;

Reference yield:

: 104-13-2
4-Butylaniline

: 1183950-19-7
methyl 2-amino-5-butylbenzoate

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine / 4 h / 0 - 90 °C / Inert atmosphere

2: bromine; acetic acid / 3 h / 0 - 80 °C / Inert atmosphere

3: 1-methyl-pyrrolidin-2-one / 3 h / 140 °C / Inert atmosphere

4: water; sulfuric acid; acetic acid / 3 h / 90 °C / Inert atmosphere

5: thionyl chloride / 3 h / 0 - 90 °C / Inert atmosphere

With pyridine; thionyl chloride; sulfuric acid; water; bromine; acetic acid; In 1-methyl-pyrrolidin-2-one;