2-(4-{[4-chloro-3-(trifluoromethyl)phenyl]oxy}phenyl)ethyl imidocarbamate triflate

Base Information

Chemical Name:2-(4-{[4-chloro-3-(trifluoromethyl)phenyl]oxy}phenyl)ethyl imidocarbamate triflate
CAS No.:1380429-44-6
Molecular Formula:CHF₃O₃S*C₁₆H₁₄ClF₃N₂O₂
Molecular Weight:508.826
Hs Code.:

Synonyms:2-(4-{[4-chloro-3-(trifluoromethyl)phenyl]oxy}phenyl)ethyl imidocarbamate triflate

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Chemical Property of 2-(4-{[4-chloro-3-(trifluoromethyl)phenyl]oxy}phenyl)ethyl imidocarbamate triflate

Chemical Property:

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Technology Process of 2-(4-{[4-chloro-3-(trifluoromethyl)phenyl]oxy}phenyl)ethyl imidocarbamate triflate

There total 5 articles about 2-(4-{[4-chloro-3-(trifluoromethyl)phenyl]oxy}phenyl)ethyl imidocarbamate triflate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.8%

: 420-04-2
CYANAMID

: 1493-13-6
trifluorormethanesulfonic acid

: 1369254-76-1
2-(4-{[4-chloro-3-(trifluoromethyl)phenyl]oxy}phenyl)ethanol

: 1380429-44-6
2-(4-{[4-chloro-3-(trifluoromethyl)phenyl]oxy}phenyl)ethyl imidocarbamate triflate

Guidance literature:: In tetrahydrofuran; at 55 ℃; for 3h; Inert atmosphere;

Reference yield:

: 6294-93-5
4-chloro-3-trifluoromethylphenol

: 1380429-44-6
2-(4-{[4-chloro-3-(trifluoromethyl)phenyl]oxy}phenyl)ethyl imidocarbamate triflate

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 0.33 h / 120 °C / Microwave irradiation

2.1: sodium hydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

2.2: 20 °C

3.1: 9-borabicyclo[3.3.1]nonane / tetrahydrofuran / 0 - 20 °C

3.2: 2 h / 50 °C

4.1: tetrahydrofuran / 3 h / 55 °C / Inert atmosphere

With sodium hydride; potassium carbonate; 9-borabicyclo[3.3.1]nonane; In tetrahydrofuran; N,N-dimethyl-formamide; 2.1: Wittig Reaction;

Reference yield:

: 516481-95-1
4-{[4-chloro-3-(trifluoromethyl)phenyl]oxy}benzaldehyde

: 1380429-44-6
2-(4-{[4-chloro-3-(trifluoromethyl)phenyl]oxy}phenyl)ethyl imidocarbamate triflate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

1.2: 20 °C

2.1: 9-borabicyclo[3.3.1]nonane / tetrahydrofuran / 0 - 20 °C

2.2: 2 h / 50 °C

3.1: tetrahydrofuran / 3 h / 55 °C / Inert atmosphere

With sodium hydride; 9-borabicyclo[3.3.1]nonane; In tetrahydrofuran; 1.1: Wittig Reaction;