[N-(tert-Butyloxycarbonyl)-N-(2-propen-1-yl)amino]-2-iodo-3-(methoxymethoxy)benzene

Base Information

Chemical Name:[N-(tert-Butyloxycarbonyl)-N-(2-propen-1-yl)amino]-2-iodo-3-(methoxymethoxy)benzene
CAS No.:198708-88-2
Molecular Formula:C₁₆H₂₂INO₄
Molecular Weight:419.259
Hs Code.:

Synonyms:[N-(tert-Butyloxycarbonyl)-N-(2-propen-1-yl)amino]-2-iodo-3-(methoxymethoxy)benzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [N-(tert-Butyloxycarbonyl)-N-(2-propen-1-yl)amino]-2-iodo-3-(methoxymethoxy)benzene

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Technology Process of [N-(tert-Butyloxycarbonyl)-N-(2-propen-1-yl)amino]-2-iodo-3-(methoxymethoxy)benzene

There total 6 articles about [N-(tert-Butyloxycarbonyl)-N-(2-propen-1-yl)amino]-2-iodo-3-(methoxymethoxy)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 144-55-8
sodium hydrogencarbonate

: 106-95-6
allyl bromide

: 198708-87-1
[N-(tert-Butyloxycarbonyl)amino]-2-iodo-3-(methoxymethoxy)benzene

: 198708-88-2
[N-(tert-Butyloxycarbonyl)-N-(2-propen-1-yl)amino]-2-iodo-3-(methoxymethoxy)benzene

Guidance literature:: With NaH; In N,N-dimethyl-formamide;

Reference yield:

: 554-84-7
meta-nitrophenol

: 198708-88-2
[N-(tert-Butyloxycarbonyl)-N-(2-propen-1-yl)amino]-2-iodo-3-(methoxymethoxy)benzene

Guidance literature:: Multi-step reaction with 5 steps

1: 89 percent / NaH, Bu₄NI

2: 89 percent / Al-Hg / diethyl ether; H₂O

4: 1.) n-BuLi, TMEDA, 2.) ICH₂CH₂Cl / 1.) THF, -20 deg C, 2 h

5: NaH

With n-butyllithium; 1-chloro-2-iodoethane; N,N,N,N,-tetramethylethylenediamine; aluminium amalgam; tetra-(n-butyl)ammonium iodide; sodium hydride; In diethyl ether; water;
DOI:10.1021/jo971686p

Reference yield:

: 25458-48-4
1-(methoxymethoxy)-3-nitrobenzene

: 198708-88-2
[N-(tert-Butyloxycarbonyl)-N-(2-propen-1-yl)amino]-2-iodo-3-(methoxymethoxy)benzene

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / Al-Hg / diethyl ether; H₂O

3: 1.) n-BuLi, TMEDA, 2.) ICH₂CH₂Cl / 1.) THF, -20 deg C, 2 h

4: NaH

With n-butyllithium; 1-chloro-2-iodoethane; N,N,N,N,-tetramethylethylenediamine; aluminium amalgam; sodium hydride; In diethyl ether; water;
DOI:10.1021/jo971686p