6,6'-((ethane-1,2-diylbis(benzylazanediyl))bis(methylene))dipicolinic acid

Base Information

Chemical Name:6,6'-((ethane-1,2-diylbis(benzylazanediyl))bis(methylene))dipicolinic acid
CAS No.:1332367-80-2
Molecular Formula:C₃₀H₃₀N₄O₄
Molecular Weight:510.593
Hs Code.:

Synonyms:6,6'-((ethane-1,2-diylbis(benzylazanediyl))bis(methylene))dipicolinic acid

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Chemical Property of 6,6'-((ethane-1,2-diylbis(benzylazanediyl))bis(methylene))dipicolinic acid

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Technology Process of 6,6'-((ethane-1,2-diylbis(benzylazanediyl))bis(methylene))dipicolinic acid

There total 6 articles about 6,6'-((ethane-1,2-diylbis(benzylazanediyl))bis(methylene))dipicolinic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1332367-79-9
dimethyl 6,6′([ethane-1,2-diylbis{benzylazanediyl}]bis[methylene])dipicolinate

: 1332367-80-2
6,6'-((ethane-1,2-diylbis(benzylazanediyl))bis(methylene))dipicolinic acid

Guidance literature:: With water; lithium hydroxide; In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.1016/j.bioorg.2020.103965

Reference yield: 85.0%

: 1332367-80-2
6,6'-((ethane-1,2-diylbis(benzylazanediyl))bis(methylene))dipicolinic acid

Guidance literature:

Reference yield:

: 100-52-7
benzaldehyde

: 1332367-80-2
6,6'-((ethane-1,2-diylbis(benzylazanediyl))bis(methylene))dipicolinic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: methanol / 12 h / 75 °C / Inert atmosphere

1.2: 0 - 20 °C / Inert atmosphere

2.1: alkali metal carbonate / acetonitrile / 60 °C

3.1: water; lithium hydroxide / tetrahydrofuran / 2 h / 20 °C

With water; lithium hydroxide; In tetrahydrofuran; methanol; acetonitrile;
DOI:10.1016/j.bioorg.2020.103965