S-(3-nitrophenyl)benzenethiosulfonate

Base Information Edit

Chemical Name:S-(3-nitrophenyl)benzenethiosulfonate
CAS No.:95533-72-5
Molecular Formula:C₁₂H₉NO₄S₂
Molecular Weight:295.34
Hs Code.:
Mol file:95533-72-5.mol

Synonyms:S-(3-nitrophenyl)benzenethiosulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of S-(3-nitrophenyl)benzenethiosulfonate Edit

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Technology Process of S-(3-nitrophenyl)benzenethiosulfonate

There total 4 articles about S-(3-nitrophenyl)benzenethiosulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 537-91-7
bis(3-nitrophenyl) disulfide

: 873-55-2
sodium benzenesulfonate

: 95533-72-5
S-(3-nitrophenyl)benzenethiosulfonate

Guidance literature:: With N-Bromosuccinimide; In acetonitrile; at 25 ℃; for 6h;
DOI:10.1002/cjoc.201200028

Reference yield:

: 98-09-9
benzenesulfonyl chloride

: 95533-72-5
S-(3-nitrophenyl)benzenethiosulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium sulfite; sodium hydrogencarbonate / water / 4 h / 80 °C

2: N-Bromosuccinimide / acetonitrile / 20 °C

With N-Bromosuccinimide; sodium hydrogencarbonate; sodium sulfite; In water; acetonitrile;
DOI:10.1021/acs.orglett.0c02370