Technology Process of C26H24ClN7O2
There total 6 articles about C26H24ClN7O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
N-ethyl-N,N-diisopropylamine;
In
isopropyl alcohol;
at 80 ℃;
for 36h;
Inert atmosphere;
Sealed tube;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 1,4-dioxane / 4.5 h / 40 - 100 °C
2.1: 4-methyl-morpholine; isobutyl chloroformate / tetrahydrofuran / 1 h / -15 °C
2.2: 21 - 60 °C
3.1: triethylamine; chloro-trimethyl-silane / acetonitrile / 48 h / 90 °C / Inert atmosphere
4.1: trifluoroacetic acid / dichloromethane / 2 h / 21 °C
5.1: N-ethyl-N,N-diisopropylamine / isopropyl alcohol / 36 h / 80 °C / Inert atmosphere; Sealed tube
With
4-methyl-morpholine; chloro-trimethyl-silane; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; isobutyl chloroformate;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; isopropyl alcohol; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 4-methyl-morpholine; isobutyl chloroformate / tetrahydrofuran / 1 h / -15 °C
1.2: 21 - 60 °C
2.1: triethylamine; chloro-trimethyl-silane / acetonitrile / 48 h / 90 °C / Inert atmosphere
3.1: trifluoroacetic acid / dichloromethane / 2 h / 21 °C
4.1: N-ethyl-N,N-diisopropylamine / isopropyl alcohol / 36 h / 80 °C / Inert atmosphere; Sealed tube
With
4-methyl-morpholine; chloro-trimethyl-silane; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; isobutyl chloroformate;
In
tetrahydrofuran; dichloromethane; isopropyl alcohol; acetonitrile;