(2Z)-3-(4-benzyloxy-3,5-dimethyl-phenyl)-2-(tetrahydro-pyran-2-yloxy)acrylic acid monopotassium salt

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Chemical Name:(2Z)-3-(4-benzyloxy-3,5-dimethyl-phenyl)-2-(tetrahydro-pyran-2-yloxy)acrylic acid monopotassium salt
CAS No.:1117699-25-8
Molecular Formula:C₂₃H₂₅O₅*K
Molecular Weight:420.547
Hs Code.:

Synonyms:(2Z)-3-(4-benzyloxy-3,5-dimethyl-phenyl)-2-(tetrahydro-pyran-2-yloxy)acrylic acid monopotassium salt

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Chemical Property of (2Z)-3-(4-benzyloxy-3,5-dimethyl-phenyl)-2-(tetrahydro-pyran-2-yloxy)acrylic acid monopotassium salt

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Technology Process of (2Z)-3-(4-benzyloxy-3,5-dimethyl-phenyl)-2-(tetrahydro-pyran-2-yloxy)acrylic acid monopotassium salt

There total 3 articles about (2Z)-3-(4-benzyloxy-3,5-dimethyl-phenyl)-2-(tetrahydro-pyran-2-yloxy)acrylic acid monopotassium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1117699-24-7
ethyl (2Z)-3-(4-benzyloxy-3,5-dimethyl-phenyl)-2-(tetrahydropyran-2-yloxy)acrylate

: 1117699-25-8
(2Z)-3-(4-benzyloxy-3,5-dimethyl-phenyl)-2-(tetrahydro-pyran-2-yloxy)acrylic acid monopotassium salt

Guidance literature:: With potassium hydroxide; In tert-Amyl alcohol; for 1h; Product distribution / selectivity; Reflux; Industrial scale;

Reference yield:

: 110-87-2
3,4-dihydro-2H-pyran

: 1117699-25-8
(2Z)-3-(4-benzyloxy-3,5-dimethyl-phenyl)-2-(tetrahydro-pyran-2-yloxy)acrylic acid monopotassium salt

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / toluene / 20 °C / Industrial scale

2: potassium 2-methylbutan-2-olate / tetrahydrofuran / 20 °C / Industrial scale

3: potassium hydroxide / tert-Amyl alcohol / 1 h / Reflux; Industrial scale

With potassium 2-methylbutan-2-olate; potassium hydroxide; toluene-4-sulfonic acid; In tetrahydrofuran; tert-Amyl alcohol; toluene;

Reference yield:

: 61675-94-3
ethyl (tetrahydropyranyloxy)acetate

: 1117699-25-8
(2Z)-3-(4-benzyloxy-3,5-dimethyl-phenyl)-2-(tetrahydro-pyran-2-yloxy)acrylic acid monopotassium salt

Guidance literature:: Multi-step reaction with 2 steps

1: potassium 2-methylbutan-2-olate / tetrahydrofuran / 20 °C / Industrial scale

2: potassium hydroxide / tert-Amyl alcohol / 1 h / Reflux; Industrial scale

With potassium 2-methylbutan-2-olate; potassium hydroxide; In tetrahydrofuran; tert-Amyl alcohol;