1,3-dicyclohexylimidazolium perchlorate

Base Information

• Chemical Name: 1,3-dicyclohexylimidazolium perchlorate
• CAS No.: 1431142-90-3
• Molecular Formula: C₁₅H₂₅N₂*ClO₄
• Molecular Weight: 332.827
• Mol file: 1431142-90-3.mol

Synonyms:1,3-dicyclohexylimidazolium perchlorate

Chemical Property of 1,3-dicyclohexylimidazolium perchlorate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,3-dicyclohexylimidazolium perchlorate

There total 4 articles about 1,3-dicyclohexylimidazolium perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

N,N'-dicyclohexylethylenediimine (3673-06-1) + acetic acid (64-19-7,77671-22-8) → 1,3-dicyclohexylimidazolium perchlorate (1431142-90-3)

Guidance literature:

N,N'-dicyclohexylethylenediimine; acetic acid; With perchloric acid; at 20 ℃;

In ethanol; Reflux;

DOI:10.1134/S1070363217120489

Reference yield: 98.0%

1,3-dicyclohexyl-2-formylimidazolium perchlorate (1431142-86-7) → 1,3-dicyclohexylimidazolium perchlorate (1431142-90-3)

Guidance literature:

In ethanol; Reflux;

DOI:10.1139/cjc-2012-0497

Reference yield:

N,N'-dicyclohexylethylenediimine (3673-06-1) → 1,3-dicyclohexylimidazolium perchlorate (1431142-90-3)

Guidance literature:

Multi-step reaction with 2 steps

1: perchloric acid

2: ethanol / Reflux

With perchloric acid; In ethanol;

DOI:10.1139/cjc-2012-0497

upstream raw materials:

1,3-dicyclohexyl-2-formylimidazolium perchlorate

N,N'-dicyclohexylethylenediimine

acetic acid

cyclohexylamine