9-(4-fluorophenethyl)-6-chloro-2,3,4,9-tetrahydro-2-methyl-1H-pyrido[3,4-b]indole

Base Information

Chemical Name:9-(4-fluorophenethyl)-6-chloro-2,3,4,9-tetrahydro-2-methyl-1H-pyrido[3,4-b]indole
CAS No.:1189798-80-8
Molecular Formula:C₂₀H₂₀ClFN₂
Molecular Weight:342.844
Hs Code.:

Synonyms:9-(4-fluorophenethyl)-6-chloro-2,3,4,9-tetrahydro-2-methyl-1H-pyrido[3,4-b]indole

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Chemical Property of 9-(4-fluorophenethyl)-6-chloro-2,3,4,9-tetrahydro-2-methyl-1H-pyrido[3,4-b]indole

Chemical Property:

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Technology Process of 9-(4-fluorophenethyl)-6-chloro-2,3,4,9-tetrahydro-2-methyl-1H-pyrido[3,4-b]indole

There total 3 articles about 9-(4-fluorophenethyl)-6-chloro-2,3,4,9-tetrahydro-2-methyl-1H-pyrido[3,4-b]indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1189798-82-0
2-(1-(4-fluorophenethyl)-5-chloro-1H-indol-3-yl)-N-methylethanamine

: 1189798-80-8
9-(4-fluorophenethyl)-6-chloro-2,3,4,9-tetrahydro-2-methyl-1H-pyrido[3,4-b]indole

Guidance literature:: 2-(1-(4-fluorophenethyl)-5-chloro-1H-indol-3-yl)-N-methylethanamine; With trifluoroacetic acid; In acetonitrile; Reflux;

formaldehyd; In water; acetonitrile; for 0.25 - 0.333333h; Reflux;

With sodium hydrogencarbonate; In water; ethyl acetate; at 25 ℃;

Reference yield:

: 1189785-82-7
1-(4-fluorophenethyl)-1-(4-chlorophenyl)hydrazine

: 1189798-80-8
9-(4-fluorophenethyl)-6-chloro-2,3,4,9-tetrahydro-2-methyl-1H-pyrido[3,4-b]indole

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride / 1,4-dioxane; ethyl acetate

1.2: 25 - 80 °C

2.1: trifluoroacetic acid / acetonitrile / Reflux

2.2: 0.25 - 0.33 h / Reflux

2.3: 25 °C

With hydrogenchloride; trifluoroacetic acid; In 1,4-dioxane; ethyl acetate; acetonitrile;

Reference yield:

: 1073-70-7
4-chlorophenylhydrazine hydrochloride

: 1189798-80-8
9-(4-fluorophenethyl)-6-chloro-2,3,4,9-tetrahydro-2-methyl-1H-pyrido[3,4-b]indole

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrabutyl-ammonium chloride; sodium hydroxide / water / 3.5 h / 75 - 80 °C

2.1: hydrogenchloride / 1,4-dioxane; ethyl acetate

2.2: 25 - 80 °C

3.1: trifluoroacetic acid / acetonitrile / Reflux

3.2: 0.25 - 0.33 h / Reflux

3.3: 25 °C

With hydrogenchloride; tetrabutyl-ammonium chloride; trifluoroacetic acid; sodium hydroxide; In 1,4-dioxane; water; ethyl acetate; acetonitrile;