[1-(2-methoxyethyl)-4,4-dimethyl-2-oxopyrrolidin-3-yl] 4-methylcyclohex-3-ene-1-carboxylate

Base Information

Chemical Name:[1-(2-methoxyethyl)-4,4-dimethyl-2-oxopyrrolidin-3-yl] 4-methylcyclohex-3-ene-1-carboxylate
CAS No.:737762-31-1
Molecular Formula:C₁₇H₂₇NO₄
Molecular Weight:309.406
Hs Code.:

Synonyms:[1-(2-methoxyethyl)-4,4-dimethyl-2-oxopyrrolidin-3-yl] 4-methylcyclohex-3-ene-1-carboxylate

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Chemical Property of [1-(2-methoxyethyl)-4,4-dimethyl-2-oxopyrrolidin-3-yl] 4-methylcyclohex-3-ene-1-carboxylate

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Technology Process of [1-(2-methoxyethyl)-4,4-dimethyl-2-oxopyrrolidin-3-yl] 4-methylcyclohex-3-ene-1-carboxylate

There total 6 articles about [1-(2-methoxyethyl)-4,4-dimethyl-2-oxopyrrolidin-3-yl] 4-methylcyclohex-3-ene-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 78-79-5,9003-31-0
isoprene

: 737762-21-9
(+/-)-[1-(2-methoxyethyl)-4,4-dimethyl-2-oxopyrrolidin-3-yl] acrylate

: 737762-31-1
[1-(2-methoxyethyl)-4,4-dimethyl-2-oxopyrrolidin-3-yl] 4-methylcyclohex-3-ene-1-carboxylate

Guidance literature:: With titanium tetrachloride; In dichloromethane; at -20 - 0 ℃; for 41h;
DOI:10.1002/ejoc.200400019

Reference yield:

: 117895-47-3
3-(benzyloxy)-4,4-dimethyldihydrofuran-2(3H)-one

: 737762-31-1
[1-(2-methoxyethyl)-4,4-dimethyl-2-oxopyrrolidin-3-yl] 4-methylcyclohex-3-ene-1-carboxylate

Guidance literature:: Multi-step reaction with 5 steps

1: NH₃ / H₂O / 230 °C

2: 87 percent / NaH / dimethylformamide / 12 h / 20 °C

3: 100 percent / H₂ / Pd(OH)2/C / ethyl acetate / 5 h / 20 °C

4: 52 percent / triethylamine / CH₂Cl₂ / 2 h / -20 °C

5: 90 percent / TiCl₄ / CH₂Cl₂ / 41 h / -20 - 0 °C

With ammonia; hydrogen; titanium tetrachloride; sodium hydride; triethylamine; palladium dihydroxide; In dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; 5: Diels-Alder reaction;
DOI:10.1002/ejoc.200400019

Reference yield:

: 79-50-5
pantolactone

: 737762-31-1
[1-(2-methoxyethyl)-4,4-dimethyl-2-oxopyrrolidin-3-yl] 4-methylcyclohex-3-ene-1-carboxylate

Guidance literature:: Multi-step reaction with 6 steps

1: Cs₂CO₃ / dimethylformamide

2: NH₃ / H₂O / 230 °C

3: 87 percent / NaH / dimethylformamide / 12 h / 20 °C

4: 100 percent / H₂ / Pd(OH)2/C / ethyl acetate / 5 h / 20 °C

5: 52 percent / triethylamine / CH₂Cl₂ / 2 h / -20 °C

6: 90 percent / TiCl₄ / CH₂Cl₂ / 41 h / -20 - 0 °C

With ammonia; hydrogen; titanium tetrachloride; sodium hydride; caesium carbonate; triethylamine; palladium dihydroxide; In dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; 6: Diels-Alder reaction;
DOI:10.1002/ejoc.200400019