N-[(6β,14β-epoxy-17-isobutyl-3-methoxymorphinan-6α-yl)methyl]-4-methoxybenzamide

Base Information

Chemical Name:N-[(6β,14β-epoxy-17-isobutyl-3-methoxymorphinan-6α-yl)methyl]-4-methoxybenzamide
CAS No.:1272675-72-5
Molecular Formula:C₃₀H₃₈N₂O₄
Molecular Weight:490.643
Hs Code.:

Synonyms:N-[(6β,14β-epoxy-17-isobutyl-3-methoxymorphinan-6α-yl)methyl]-4-methoxybenzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[(6β,14β-epoxy-17-isobutyl-3-methoxymorphinan-6α-yl)methyl]-4-methoxybenzamide

Chemical Property:

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Technology Process of N-[(6β,14β-epoxy-17-isobutyl-3-methoxymorphinan-6α-yl)methyl]-4-methoxybenzamide

There total 2 articles about N-[(6β,14β-epoxy-17-isobutyl-3-methoxymorphinan-6α-yl)methyl]-4-methoxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1130020-76-6
(6β,14β-epoxy-17-isobutyl-3-methoxymorphinan-6α-yl)methanamine

: 100-07-2
4-methoxy-benzoyl chloride

: 1272675-72-5
N-[(6β,14β-epoxy-17-isobutyl-3-methoxymorphinan-6α-yl)methyl]-4-methoxybenzamide

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 ℃; Inert atmosphere;
DOI:10.1016/j.bmc.2010.12.035

Reference yield:

: 1103501-77-4
C₂₂H₂₈N₄O₂

: 1272675-72-5
N-[(6β,14β-epoxy-17-isobutyl-3-methoxymorphinan-6α-yl)methyl]-4-methoxybenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: platinum(IV) oxide; camphor-10-sulfonic acid; hydrogen / methanol / 96 h / 20 °C

2: triethylamine / tetrahydrofuran / 0 °C / Inert atmosphere

With platinum(IV) oxide; camphor-10-sulfonic acid; hydrogen; triethylamine; In tetrahydrofuran; methanol;
DOI:10.1016/j.bmc.2010.12.035