N⁴-benzoyl-3',5'-bis-O-(tert-butyldimethylsilyl)-6-vinyl-2'-deoxycitidine

Base Information

Chemical Name:N⁴-benzoyl-3',5'-bis-O-(tert-butyldimethylsilyl)-6-vinyl-2'-deoxycitidine
CAS No.:927652-17-3
Molecular Formula:C₃₀H₄₇N₃O₅Si₂
Molecular Weight:585.891
Hs Code.:

N<sup>4</sup>-benzoyl-3',5'-bis-O-(tert-butyldimethylsilyl)-6-vinyl-2'-deoxycitidine

Synonyms:N⁴-benzoyl-3',5'-bis-O-(tert-butyldimethylsilyl)-6-vinyl-2'-deoxycitidine

Suppliers and Price of N⁴-benzoyl-3',5'-bis-O-(tert-butyldimethylsilyl)-6-vinyl-2'-deoxycitidine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N⁴-benzoyl-3',5'-bis-O-(tert-butyldimethylsilyl)-6-vinyl-2'-deoxycitidine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N⁴-benzoyl-3',5'-bis-O-(tert-butyldimethylsilyl)-6-vinyl-2'-deoxycitidine

There total 1 articles about N⁴-benzoyl-3',5'-bis-O-(tert-butyldimethylsilyl)-6-vinyl-2'-deoxycitidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 927652-16-2
N⁴-benzoyl-3',5'-bis-O-(tert-butyldimethylsilyl)-6-formyl-2'-deoxycytidine

: 1779-49-3
Methyltriphenylphosphonium bromide

: 927652-17-3
N⁴-benzoyl-3',5'-bis-O-(tert-butyldimethylsilyl)-6-vinyl-2'-deoxycitidine

Guidance literature:: Methyltriphenylphosphonium bromide; With n-butyllithium; In tetrahydrofuran; at 0 ℃; for 0.5h;

N⁴-benzoyl-3',5'-bis-O-(tert-butyldimethylsilyl)-6-formyl-2'-deoxycytidine; In tetrahydrofuran; at 20 ℃; for 1h; Further stages.;
DOI:10.3987/com-06-s(o)3

Reference yield: 85.0%

: 927652-17-3
N⁴-benzoyl-3',5'-bis-O-(tert-butyldimethylsilyl)-6-vinyl-2'-deoxycitidine

: 75-08-1
ethanethiol

: N⁴-benzoyl-3',5'-bis-O-(tert-butyldimethylsilyl)-6-{1-[2-(ethylthio)]ethyl}-2'-deoxycytidine

Guidance literature:: In dichloromethane; at 20 ℃; for 1h;
DOI:10.3987/com-06-s(o)3

Reference yield:

: 927652-17-3
N⁴-benzoyl-3',5'-bis-O-(tert-butyldimethylsilyl)-6-vinyl-2'-deoxycitidine

: N⁴-benzoyl-6-{1-[2-(ethylthio)]ethyl}-2'-deoxycytidine

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / CH₂Cl₂ / 1 h / 20 °C

2: 79 percent / tetrabutylammonium fluoride / tetrahydrofuran / 4 h / 20 °C

With tetrabutyl ammonium fluoride; In tetrahydrofuran; dichloromethane;
DOI:10.3987/com-06-s(o)3