Carbonic acid (2S,4R,5R)-4-hydroxy-5-{6-[2-(4-nitro-phenyl)-ethoxycarbonylamino]-purin-9-yl}-tetrahydro-furan-2-ylmethyl ester 2-(4-nitro-phenyl)-ethyl ester

Base Information

Chemical Name:Carbonic acid (2S,4R,5R)-4-hydroxy-5-{6-[2-(4-nitro-phenyl)-ethoxycarbonylamino]-purin-9-yl}-tetrahydro-furan-2-ylmethyl ester 2-(4-nitro-phenyl)-ethyl ester
CAS No.:177084-28-5
Molecular Formula:C₂₈H₂₇N₇O₁₁
Molecular Weight:637.563
Hs Code.:

Carbonic acid (2S,4R,5R)-4-hydroxy-5-{6-[2-(4-nitro-phenyl)-ethoxycarbonylamino]-purin-9-yl}-tetrahydro-furan-2-ylmethyl ester 2-(4-nitro-phenyl)-ethyl ester

Synonyms:Carbonic acid (2S,4R,5R)-4-hydroxy-5-{6-[2-(4-nitro-phenyl)-ethoxycarbonylamino]-purin-9-yl}-tetrahydro-furan-2-ylmethyl ester 2-(4-nitro-phenyl)-ethyl ester

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Chemical Property of Carbonic acid (2S,4R,5R)-4-hydroxy-5-{6-[2-(4-nitro-phenyl)-ethoxycarbonylamino]-purin-9-yl}-tetrahydro-furan-2-ylmethyl ester 2-(4-nitro-phenyl)-ethyl ester

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Technology Process of Carbonic acid (2S,4R,5R)-4-hydroxy-5-{6-[2-(4-nitro-phenyl)-ethoxycarbonylamino]-purin-9-yl}-tetrahydro-furan-2-ylmethyl ester 2-(4-nitro-phenyl)-ethyl ester

There total 5 articles about Carbonic acid (2S,4R,5R)-4-hydroxy-5-{6-[2-(4-nitro-phenyl)-ethoxycarbonylamino]-purin-9-yl}-tetrahydro-furan-2-ylmethyl ester 2-(4-nitro-phenyl)-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 88091-68-3
2-(4-nitrophenyl)ethoxycarbonyl chloride

: 112237-60-2
3'-deoxy-N⁶-<2-(4-nitrophenyl)ethoxycarbonyl>adenosine

: 177084-28-5
Carbonic acid (2S,4R,5R)-4-hydroxy-5-{6-[2-(4-nitro-phenyl)-ethoxycarbonylamino]-purin-9-yl}-tetrahydro-furan-2-ylmethyl ester 2-(4-nitro-phenyl)-ethyl ester

Guidance literature:: In pyridine; dichloromethane; at -10 ℃; for 1.66667h;
DOI:10.1002/hlca.19960790304

Reference yield: 6.0%

: 88091-68-3
2-(4-nitrophenyl)ethoxycarbonyl chloride

: 112237-60-2
3'-deoxy-N⁶-<2-(4-nitrophenyl)ethoxycarbonyl>adenosine

: 177084-28-5
Carbonic acid (2S,4R,5R)-4-hydroxy-5-{6-[2-(4-nitro-phenyl)-ethoxycarbonylamino]-purin-9-yl}-tetrahydro-furan-2-ylmethyl ester 2-(4-nitro-phenyl)-ethyl ester

: Carbonic acid (2R,3R,5S)-2-{6-[2-(4-nitro-phenyl)-ethoxycarbonylamino]-purin-9-yl}-5-[2-(4-nitro-phenyl)-ethoxycarbonyloxymethyl]-tetrahydro-furan-3-yl ester 2-(4-nitro-phenyl)-ethyl ester

: 7,8-dihydro-N⁶,7,2'-O-tris[2-(4-nitrophenyl)ethoxycarbonyl]-8,5'-O-cyclocordycepin

Guidance literature:: With pyridine; -30 deg C, 30 min and 100 min, -10 deg C;
DOI:10.1002/hlca.19960790210

Reference yield:

: 88091-70-7
1-methyl-3-[2-(4-nitrophenyl)ethoxycarbonyl]imidazolium chloride

: 177084-28-5
Carbonic acid (2S,4R,5R)-4-hydroxy-5-{6-[2-(4-nitro-phenyl)-ethoxycarbonylamino]-purin-9-yl}-tetrahydro-furan-2-ylmethyl ester 2-(4-nitro-phenyl)-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / CH₂Cl₂ / 40 h / Ambient temperature

2: 87 percent / K₂CO₃ / methanol / 3 h / Ambient temperature

3: 73 percent / pyridine / -30 deg C, 30 min and 100 min, -10 deg C

With pyridine; potassium carbonate; In methanol; dichloromethane;
DOI:10.1002/hlca.19960790210