Methyl 4-{[(tert-butoxycarbonyl)(1H-imidazol-2-ylmethyl)amino]methyl}benzoate

Base Information

• Chemical Name: Methyl 4-{[(tert-butoxycarbonyl)(1H-imidazol-2-ylmethyl)amino]methyl}benzoate
• CAS No.: 675137-08-3
• Molecular Formula: C₁₈H₂₃N₃O₄
• Molecular Weight: 345.398

Synonyms:Methyl 4-{[(tert-butoxycarbonyl)(1H-imidazol-2-ylmethyl)amino]methyl}benzoate

Chemical Property of Methyl 4-{[(tert-butoxycarbonyl)(1H-imidazol-2-ylmethyl)amino]methyl}benzoate

Chemical Property:

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Technology Process of Methyl 4-{[(tert-butoxycarbonyl)(1H-imidazol-2-ylmethyl)amino]methyl}benzoate

There total 4 articles about Methyl 4-{[(tert-butoxycarbonyl)(1H-imidazol-2-ylmethyl)amino]methyl}benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Ethyl 3-(2-{[{4-[(8-cyclohexyl-2,8-diazaspiro[4.5]dec-2-yl)methyl]benzoyl}(1H-imidazol-2-ylmethyl)amino]methyl}-1H-imidazol-1-yl)propanoate (957778-75-5) + di-tert-butyl dicarbonate (24424-99-5) → Methyl 4-{[(tert-butoxycarbonyl)(1H-imidazol-2-ylmethyl)amino]methyl}benzoate (675137-08-3)

Guidance literature:

With triethylamine; hydroxylamine hydrochloride; In tetrahydrofuran; at 20 ℃; for 14h;

Reference yield:

4-(1H-imidazol-2-ylmethylaminomethyl)-benzoic acid methyl ester (369656-39-3) + di-tert-butyl dicarbonate (24424-99-5) → Methyl 4-{[(tert-butoxycarbonyl)(1H-imidazol-2-ylmethyl)amino]methyl}benzoate (675137-08-3)

Guidance literature:

In DMF (N,N-dimethyl-formamide); at 20 ℃; for 1h;

Reference yield:

methanol (67-56-1) + 4-{[(tert-butoxycarbonyl)(1H-imidazol-2-ylmethyl)amino]methyl}benzoic acid (369656-38-2) → Methyl 4-{[(tert-butoxycarbonyl)(1H-imidazol-2-ylmethyl)amino]methyl}benzoate (675137-08-3)

Guidance literature:

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; at 20 ℃;

upstream raw materials:

4-(1H-imidazol-2-ylmethylaminomethyl)-benzoic acid methyl ester

di-tert-butyl dicarbonate

methanol

4-{[(tert-butoxycarbonyl)(1H-imidazol-2-ylmethyl)amino]methyl}benzoic acid

Downstream raw materials:

4-{[N-boc(N-1H-imidazol-2-ylmethyl)amino]methyl} benzyl alcohol

4-{[(tert-butoxycarbonyl)(1H-imidazol-2-ylmethyl)amino]methyl}benzoic acid

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