5-acetyl-6-methyl-2-oxo-4-phenyl-1,2,3,4-tetrahydro-pyridine-3-carbonitrile

Base Information

Chemical Name:5-acetyl-6-methyl-2-oxo-4-phenyl-1,2,3,4-tetrahydro-pyridine-3-carbonitrile
CAS No.:117226-91-2
Molecular Formula:C₁₅H₁₄N₂O₂
Molecular Weight:254.288
Hs Code.:

Synonyms:5-acetyl-6-methyl-2-oxo-4-phenyl-1,2,3,4-tetrahydro-pyridine-3-carbonitrile

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Chemical Property of 5-acetyl-6-methyl-2-oxo-4-phenyl-1,2,3,4-tetrahydro-pyridine-3-carbonitrile

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Technology Process of 5-acetyl-6-methyl-2-oxo-4-phenyl-1,2,3,4-tetrahydro-pyridine-3-carbonitrile

There total 3 articles about 5-acetyl-6-methyl-2-oxo-4-phenyl-1,2,3,4-tetrahydro-pyridine-3-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 100-52-7
benzaldehyde

: 123-54-6,81235-32-7
acetylacetone

: 107-91-5
cyanoacetic acid amide

: 117226-91-2
5-acetyl-6-methyl-2-oxo-4-phenyl-1,2,3,4-tetrahydro-pyridine-3-carbonitrile

Guidance literature:: With 1H-imidazole; In ethylene glycol; at 70 ℃; for 24h;
DOI:10.1002/cjoc.201200500

Reference yield: 84.0%

: 89809-89-2
5-acetyl-2-amino-3-cyano-6-methyl-4-phenyl-4H-pyran

: 117226-91-2
5-acetyl-6-methyl-2-oxo-4-phenyl-1,2,3,4-tetrahydro-pyridine-3-carbonitrile

Guidance literature:: With water; toluene-4-sulfonic acid; at 70 ℃; for 3h;
DOI:10.1016/j.tetlet.2012.06.086

Reference yield: 75.0%

: 100-52-7
benzaldehyde

: 123-54-6,81235-32-7
acetylacetone

: 109-77-3
malononitrile

: 117226-91-2
5-acetyl-6-methyl-2-oxo-4-phenyl-1,2,3,4-tetrahydro-pyridine-3-carbonitrile

Guidance literature:: With zinc dichloride modified silica sulfuric acid; In neat (no solvent); for 5h; chemoselective reaction; Reflux; Green chemistry;
DOI:10.1007/s10562-016-1806-6