(CH₃)2GeP(C₆H₅)

Base Information

• Chemical Name: (CH₃)2GeP(C₆H₅)
• CAS No.: 68160-18-9
• Molecular Formula: C₈H₁₁GeP
• Molecular Weight: 210.739
• Mol file: 68160-18-9.mol

Synonyms:(CH₃)2GeP(C₆H₅)

Chemical Property of (CH₃)2GeP(C₆H₅)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (CH₃)2GeP(C₆H₅)

There total 2 articles about (CH₃)2GeP(C₆H₅) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(phenylphosphino)-2-(dimethylbromogermyl)ethane (82312-13-8) → 2-dimethylgerma 1-phenyl phosphetane (78665-53-9) + (CH3)2GeP(C6H5) (68160-18-9) + ((CH3)2GePC6H5)2CH2CH2 (81744-50-5) + trans-3,3-dimethyl-1,2-diphenyl-1,2,3-diphosphagermolane (78665-55-1) + 3,3-dimethyl-2-(dimethylphenylgermyl)-1-phenyl-1,2,3-diphosphagermolane (82312-28-5)

Guidance literature:

With dimethyl amine; In benzene; byproducts: dimethylamine hydrobromide; Ge compd. soln. stirred at -30°C, 2-fold excess of dimethylamineallowed to bubble; centrifuged, evapd. (vac.), washed with C6H6, then with pentane, distd., obtained as mixt.;

Reference yield:

2-dimethylgerma 1-phenyl phosphetane (78665-53-9) → 3-dimethylgerma 1,2-diphenyl 1,2-diphospholane (78665-55-1) + 2,2-dimethyl-1-phenyl-germaphosphene (68160-18-9)

Guidance literature:

In not given; byproducts: CH2CH2, Ge(CH3)2; decompn. at 120°C;

Reference yield: 64.0%

(CH3)2GeP(C6H5) (68160-18-9) → dimethylgermane (1449-64-5) + phenylphosphane (638-21-1)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; Ge compd. soln. added to excess of LiAlH4 in Et2O, refluxed for 2 h; distd.;

upstream raw materials:

1-(phenylphosphino)-2-(dimethylbromogermyl)ethane

2-dimethylgerma 1-phenyl phosphetane

Downstream raw materials:

dimethylgermane

phenylphosphane