2,4,6-trimethyl-N-(2,2,2-trifluoro-1-hydroxymethylethyl)benzenesulfonamide

Base Information

Chemical Name:2,4,6-trimethyl-N-(2,2,2-trifluoro-1-hydroxymethylethyl)benzenesulfonamide
CAS No.:897380-81-3
Molecular Formula:C₁₂H₁₆F₃NO₃S
Molecular Weight:311.325
Hs Code.:

Synonyms:2,4,6-trimethyl-N-(2,2,2-trifluoro-1-hydroxymethylethyl)benzenesulfonamide

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Chemical Property of 2,4,6-trimethyl-N-(2,2,2-trifluoro-1-hydroxymethylethyl)benzenesulfonamide

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Technology Process of 2,4,6-trimethyl-N-(2,2,2-trifluoro-1-hydroxymethylethyl)benzenesulfonamide

There total 1 articles about 2,4,6-trimethyl-N-(2,2,2-trifluoro-1-hydroxymethylethyl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 897380-80-2
3,3,3-trifluoro-2-(2,4,6-trimethylbenzenesulfonylamino)propionic acid ethyl ester

: 897380-81-3
2,4,6-trimethyl-N-(2,2,2-trifluoro-1-hydroxymethylethyl)benzenesulfonamide

Guidance literature:: 3,3,3-trifluoro-2-(2,4,6-trimethylbenzenesulfonylamino)propionic acid ethyl ester; With lithium aluminium tetrahydride; In tetrahydrofuran; for 1h;

With water; In tetrahydrofuran;

Reference yield: 99.0%

: 897380-81-3
2,4,6-trimethyl-N-(2,2,2-trifluoro-1-hydroxymethylethyl)benzenesulfonamide

: 897380-82-4
1-(2,4,6-trimethylbenzenesulfonyl)-2-(trifluoromethyl)aziridine

Guidance literature:: With sodium hydride; p-toluenesulfonyl chloride; In tetrahydrofuran; at 20 ℃;

Reference yield:

: 897380-81-3
2,4,6-trimethyl-N-(2,2,2-trifluoro-1-hydroxymethylethyl)benzenesulfonamide

: 1070749-80-2
2,4,6-trimethyl-N-(2,2,2-trifluoro-1-phenylsulfanylmethylethyl)benzene-sulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride; p-toluenesulfonyl chloride / tetrahydrofuran / 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide

3.1: sodium hexamethyldisilazane / tetrahydrofuran; dimethyl sulfoxide / 0.08 h

3.2: 1 h

4.1: sodium hydride / N,N-dimethyl-formamide

With sodium hexamethyldisilazane; sodium hydride; p-toluenesulfonyl chloride; In tetrahydrofuran; dimethyl sulfoxide; N,N-dimethyl-formamide;