2,4,6-trimethyl-N-(2,2,2-trifluoro-1-phenylaminomethylethyl)benzene-sulfonamide

Base Information

Chemical Name:2,4,6-trimethyl-N-(2,2,2-trifluoro-1-phenylaminomethylethyl)benzene-sulfonamide
CAS No.:1070749-90-4
Molecular Formula:C₁₈H₂₁F₃N₂O₂S
Molecular Weight:386.438
Hs Code.:

Synonyms:2,4,6-trimethyl-N-(2,2,2-trifluoro-1-phenylaminomethylethyl)benzene-sulfonamide

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Chemical Property of 2,4,6-trimethyl-N-(2,2,2-trifluoro-1-phenylaminomethylethyl)benzene-sulfonamide

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Technology Process of 2,4,6-trimethyl-N-(2,2,2-trifluoro-1-phenylaminomethylethyl)benzene-sulfonamide

There total 6 articles about 2,4,6-trimethyl-N-(2,2,2-trifluoro-1-phenylaminomethylethyl)benzene-sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 1070749-82-4
2,4,6-trimethyl-N-(2,2,2-trifluoro-1-phenoxymethylethyl)-benzenesulfonamide

: 62-53-3
aniline

: 1070749-90-4
2,4,6-trimethyl-N-(2,2,2-trifluoro-1-phenylaminomethylethyl)benzene-sulfonamide

Guidance literature:: aniline; With sodium hexamethyldisilazane; In tetrahydrofuran; dimethyl sulfoxide; for 0.0833333h;

2,4,6-trimethyl-N-(2,2,2-trifluoro-1-phenoxymethylethyl)-benzenesulfonamide; In tetrahydrofuran; dimethyl sulfoxide; for 1h;

Reference yield:

: 897380-81-3
2,4,6-trimethyl-N-(2,2,2-trifluoro-1-hydroxymethylethyl)benzenesulfonamide

: 1070749-90-4
2,4,6-trimethyl-N-(2,2,2-trifluoro-1-phenylaminomethylethyl)benzene-sulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride; p-toluenesulfonyl chloride / tetrahydrofuran / 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide

3.1: sodium hexamethyldisilazane / tetrahydrofuran; dimethyl sulfoxide / 0.08 h

3.2: 1 h

With sodium hexamethyldisilazane; sodium hydride; p-toluenesulfonyl chloride; In tetrahydrofuran; dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: 897380-80-2
3,3,3-trifluoro-2-(2,4,6-trimethylbenzenesulfonylamino)propionic acid ethyl ester

: 1070749-90-4
2,4,6-trimethyl-N-(2,2,2-trifluoro-1-phenylaminomethylethyl)benzene-sulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h

2.1: sodium hydride; p-toluenesulfonyl chloride / tetrahydrofuran / 20 °C

3.1: sodium hydride / N,N-dimethyl-formamide

4.1: sodium hexamethyldisilazane / tetrahydrofuran; dimethyl sulfoxide / 0.08 h

4.2: 1 h

With lithium aluminium tetrahydride; sodium hexamethyldisilazane; sodium hydride; p-toluenesulfonyl chloride; In tetrahydrofuran; dimethyl sulfoxide; N,N-dimethyl-formamide;