(E)-4-trifluoromethylcinnamyl trimethylsilyl ether

Base Information

• Chemical Name: (E)-4-trifluoromethylcinnamyl trimethylsilyl ether
• CAS No.: 1000303-94-5
• Molecular Formula: C₁₃H₁₇F₃OSi
• Molecular Weight: 274.358
• Mol file: 1000303-94-5.mol

Synonyms:(E)-4-trifluoromethylcinnamyl trimethylsilyl ether

Chemical Property of (E)-4-trifluoromethylcinnamyl trimethylsilyl ether

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (E)-4-trifluoromethylcinnamyl trimethylsilyl ether

There total 1 articles about (E)-4-trifluoromethylcinnamyl trimethylsilyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-(trifluoromethyl)cinnamyl alcohol (180635-56-7) + chloro-trimethyl-silane (75-77-4) → (E)-4-trifluoromethylcinnamyl trimethylsilyl ether (1000303-94-5)

Guidance literature:

In dichloromethane;

DOI:10.1021/jo7014664

Reference yield:

(E)-4-trifluoromethylcinnamyl trimethylsilyl ether (1000303-94-5) → (E)-3-(4-trifluoromethylphenyl)-1-propenyl trimethylsilyl ether + (Z)-3-(4-trifluoromethylphenyl)-1-propenyl trimethylsilyl ether + 3-(4-trifluoromethylphenyl)propanal (166947-09-7)

Guidance literature:

In acetonitrile; at 25 ℃; for 1h; Title compound not separated from byproducts.; Irradiation;

DOI:10.1021/jo7014664

Reference yield:

(E)-4-trifluoromethylcinnamyl trimethylsilyl ether (1000303-94-5) → (E)-3-(4-trifluoromethylphenyl)-1-propenyl trimethylsilyl ether + (Z)-3-(4-trifluoromethylphenyl)-1-propenyl trimethylsilyl ether

Guidance literature:

In cyclohexane; at 25 ℃; for 1h; Title compound not separated from byproducts.; Irradiation;

DOI:10.1021/jo7014664

upstream raw materials:

p-(trifluoromethyl)cinnamyl alcohol

chloro-trimethyl-silane

Downstream raw materials:

3-(4-trifluoromethylphenyl)propanal