N,N'-(2,2'-(1,3-phenylene)bis(ethane-2,1-diyl))-bis(3,5-bis(trifluoromethyl)aniline)

Base Information

Chemical Name:N,N'-(2,2'-(1,3-phenylene)bis(ethane-2,1-diyl))-bis(3,5-bis(trifluoromethyl)aniline)
CAS No.:1228050-41-6
Molecular Formula:C₂₆H₂₀F₁₂N₂
Molecular Weight:588.439
Hs Code.:

Synonyms:N,N'-(2,2'-(1,3-phenylene)bis(ethane-2,1-diyl))-bis(3,5-bis(trifluoromethyl)aniline)

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Chemical Property of N,N'-(2,2'-(1,3-phenylene)bis(ethane-2,1-diyl))-bis(3,5-bis(trifluoromethyl)aniline)

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Technology Process of N,N'-(2,2'-(1,3-phenylene)bis(ethane-2,1-diyl))-bis(3,5-bis(trifluoromethyl)aniline)

There total 1 articles about N,N'-(2,2'-(1,3-phenylene)bis(ethane-2,1-diyl))-bis(3,5-bis(trifluoromethyl)aniline) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 328-70-1
3,6-bis(trifluoromethyl)bromobenzene

: 4289-36-5
1,3-Bis(2-aminoethyl)benzol

: 1228050-41-6
N,N'-(2,2'-(1,3-phenylene)bis(ethane-2,1-diyl))-bis(3,5-bis(trifluoromethyl)aniline)

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate; In toluene; for 72h; Inert atmosphere; Reflux;
DOI:10.1021/ic100232s

Reference yield: 74.0%

: 75-77-4
chloro-trimethyl-silane

: 1228050-41-6
N,N'-(2,2'-(1,3-phenylene)bis(ethane-2,1-diyl))-bis(3,5-bis(trifluoromethyl)aniline)

: 1228050-42-7
[3,5-CF₃NCCHCN](SiMe₃)2

Guidance literature:: N,N'-(2,2'-(1,3-phenylene)bis(ethane-2,1-diyl))-bis(3,5-bis(trifluoromethyl)aniline); With methylmagnesium chloride; In tetrahydrofuran; at -35 - 20 ℃; Inert atmosphere;

chloro-trimethyl-silane; In tetrahydrofuran; at -35 - 20 ℃; for 16h; Inert atmosphere;
DOI:10.1021/ic100232s

Reference yield: 38.0%

: 19756-04-8
tetrakis(dimethylamido)zirconium (IV)

: 1228050-41-6
N,N'-(2,2'-(1,3-phenylene)bis(ethane-2,1-diyl))-bis(3,5-bis(trifluoromethyl)aniline)

: 1228050-44-9
((μ-N,N'-(2,2'-(1,3-phenylene)bis(ethane-2,1-diyl))bis(3,5-bis(trifluoromethyl)aniline)(2-))Zr(NMe2)2NHMe2)2

Guidance literature:: In toluene; byproducts: HN(CH3)2; (inert atm.); soln. od zirconium complex in toluene was added to anilineat -35°C with stirring, warmed to room temp., stirred for 3 h; filtered, concd. in vac., crystd. from toluene, filtered, washed with cold pentane, elem. anal.;
DOI:10.1021/ic100232s