3',4'-di-O-benzyl-5,6-di-O-(p-chlorobenzoyl)-1,3,2',3'-tetraazidoneamine

Base Information

Chemical Name:3',4'-di-O-benzyl-5,6-di-O-(p-chlorobenzoyl)-1,3,2',3'-tetraazidoneamine
CAS No.:860795-33-1
Molecular Formula:C₄₀H₃₆Cl₂N₁₂O₈
Molecular Weight:883.707
Hs Code.:

Synonyms:3',4'-di-O-benzyl-5,6-di-O-(p-chlorobenzoyl)-1,3,2',3'-tetraazidoneamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3',4'-di-O-benzyl-5,6-di-O-(p-chlorobenzoyl)-1,3,2',3'-tetraazidoneamine

Chemical Property:

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Technology Process of 3',4'-di-O-benzyl-5,6-di-O-(p-chlorobenzoyl)-1,3,2',3'-tetraazidoneamine

There total 4 articles about 3',4'-di-O-benzyl-5,6-di-O-(p-chlorobenzoyl)-1,3,2',3'-tetraazidoneamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 122-01-0
4-chloro-benzoyl chloride

: 549501-27-1
3′,4′-di-O-benzyl-1,3,2′,6′-tetraazidoneamine

: 860795-33-1
3',4'-di-O-benzyl-5,6-di-O-(p-chlorobenzoyl)-1,3,2',3'-tetraazidoneamine

Guidance literature:: With triethylamine; In dichloromethane;

Reference yield:

: C₃₂H₃₈N₁₂O₆

: 860795-33-1
3',4'-di-O-benzyl-5,6-di-O-(p-chlorobenzoyl)-1,3,2',3'-tetraazidoneamine

Guidance literature:: Multi-step reaction with 2 steps

1: 4.52 g / glacial AcOH / dioxane; H₂O / 60 - 65 °C

2: 77 percent / Et₃N; DMAP / CH₂Cl₂ / Heating

With dmap; acetic acid; triethylamine; In 1,4-dioxane; dichloromethane; water;
DOI:10.1021/ol051045d

Reference yield:

: 100-39-0
benzyl bromide

: 860795-33-1
3',4'-di-O-benzyl-5,6-di-O-(p-chlorobenzoyl)-1,3,2',3'-tetraazidoneamine

Guidance literature:: Multi-step reaction with 3 steps

1: NaH; TBAI / tetrahydrofuran

2: 4.52 g / glacial AcOH / dioxane; H₂O / 60 - 65 °C

3: 77 percent / Et₃N; DMAP / CH₂Cl₂ / Heating

With dmap; tetra-(n-butyl)ammonium iodide; sodium hydride; acetic acid; triethylamine; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water;
DOI:10.1021/ol051045d