2',6'-bis(1,1-dimethylethyl)-4'-methylphenyl (2SR,3SR)-2-allyl-3-hydroxybenzenepropanoate

Base Information

Chemical Name:2',6'-bis(1,1-dimethylethyl)-4'-methylphenyl (2SR,3SR)-2-allyl-3-hydroxybenzenepropanoate
CAS No.:81835-11-2
Molecular Formula:C₂₇H₃₆O₃
Molecular Weight:408.581
Hs Code.:

Synonyms:2',6'-bis(1,1-dimethylethyl)-4'-methylphenyl (2SR,3SR)-2-allyl-3-hydroxybenzenepropanoate

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Chemical Property of 2',6'-bis(1,1-dimethylethyl)-4'-methylphenyl (2SR,3SR)-2-allyl-3-hydroxybenzenepropanoate

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Technology Process of 2',6'-bis(1,1-dimethylethyl)-4'-methylphenyl (2SR,3SR)-2-allyl-3-hydroxybenzenepropanoate

There total 3 articles about 2',6'-bis(1,1-dimethylethyl)-4'-methylphenyl (2SR,3SR)-2-allyl-3-hydroxybenzenepropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 100-52-7
benzaldehyde

: 81819-01-4
2',6'-bis(1,1-dimethylethyl)-4'-methylphenyl 4-pentenoate

: 81835-11-2
2',6'-bis(1,1-dimethylethyl)-4'-methylphenyl (2SR,3SR)-2-allyl-3-hydroxybenzenepropanoate

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; -70 degC, 6 h, then 30 min;
DOI:10.1016/S0040-4020(01)93284-3

Reference yield:

: 39716-58-0
pent-4-enoyl chloride

: 81835-11-2
2',6'-bis(1,1-dimethylethyl)-4'-methylphenyl (2SR,3SR)-2-allyl-3-hydroxybenzenepropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / n-BuLi / tetrahydrofuran; hexane / 0 °C

2: 76 percent / LDA / tetrahydrofuran / -70 degC, 6 h, then 30 min

With n-butyllithium; lithium diisopropyl amide; In tetrahydrofuran; hexane;
DOI:10.1016/S0040-4020(01)93284-3

Reference yield:

: 128-37-0
2,6-di-tert-butyl-4-methyl-phenol

: 81835-11-2
2',6'-bis(1,1-dimethylethyl)-4'-methylphenyl (2SR,3SR)-2-allyl-3-hydroxybenzenepropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / n-BuLi / tetrahydrofuran; hexane / 0 °C

2: 76 percent / LDA / tetrahydrofuran / -70 degC, 6 h, then 30 min

With n-butyllithium; lithium diisopropyl amide; In tetrahydrofuran; hexane;
DOI:10.1016/S0040-4020(01)93284-3