tert-butyl [trans-4-(4-{[(trifluoromethyl)sulfonyl]oxy}phenyl)cyclohexyl]acetate

Base Information

Chemical Name:tert-butyl [trans-4-(4-{[(trifluoromethyl)sulfonyl]oxy}phenyl)cyclohexyl]acetate
CAS No.:1166827-53-7
Molecular Formula:C₁₉H₂₅F₃O₅S
Molecular Weight:422.466
Hs Code.:

Synonyms:tert-butyl [trans-4-(4-{[(trifluoromethyl)sulfonyl]oxy}phenyl)cyclohexyl]acetate

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Chemical Property of tert-butyl [trans-4-(4-{[(trifluoromethyl)sulfonyl]oxy}phenyl)cyclohexyl]acetate

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Technology Process of tert-butyl [trans-4-(4-{[(trifluoromethyl)sulfonyl]oxy}phenyl)cyclohexyl]acetate

There total 3 articles about tert-butyl [trans-4-(4-{[(trifluoromethyl)sulfonyl]oxy}phenyl)cyclohexyl]acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 1166827-52-6
tert-butyl [trans-4-(4-hydroxyphenyl)cyclohexyl]acetate

: 1166827-53-7
tert-butyl [trans-4-(4-{[(trifluoromethyl)sulfonyl]oxy}phenyl)cyclohexyl]acetate

Guidance literature:: With pyridine; In dichloromethane; for 0.166667h; Cooling with ice;

Reference yield:

: 1166827-51-5
tert-butyl [4-(4-hydroxyphenyl)cyclohexylidene]acetate

: 1166827-53-7
tert-butyl [trans-4-(4-{[(trifluoromethyl)sulfonyl]oxy}phenyl)cyclohexyl]acetate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 3 h / 3750.38 Torr

2: pyridine / dichloromethane / 0.17 h / Cooling with ice

With pyridine; hydrogen; palladium 10% on activated carbon; In dichloromethane; ethyl acetate;

Reference yield:

: 62327-21-3
tert-butyl dimethylphosphonoacetate

: 1166827-53-7
tert-butyl [trans-4-(4-{[(trifluoromethyl)sulfonyl]oxy}phenyl)cyclohexyl]acetate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / tetrahydrofuran; mineral oil / 0 - 20 °C

2: hydrogen / palladium 10% on activated carbon / ethyl acetate / 3 h / 3750.38 Torr

3: pyridine / dichloromethane / 0.17 h / Cooling with ice

With pyridine; hydrogen; sodium hydride; palladium 10% on activated carbon; In tetrahydrofuran; dichloromethane; ethyl acetate; mineral oil;