2-{[6-(4-Acetylphenyl)hexyl]oxy}-5-[3(ethoxycarbonyl)benzoyl]benzenepropanoic acid ethyl ester

Base Information

Chemical Name:2-{[6-(4-Acetylphenyl)hexyl]oxy}-5-[3(ethoxycarbonyl)benzoyl]benzenepropanoic acid ethyl ester
CAS No.:128577-90-2
Molecular Formula:C₃₅H₄₀O₇
Molecular Weight:572.698
Hs Code.:

Synonyms:2-{[6-(4-Acetylphenyl)hexyl]oxy}-5-[3(ethoxycarbonyl)benzoyl]benzenepropanoic acid ethyl ester

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Chemical Property of 2-{[6-(4-Acetylphenyl)hexyl]oxy}-5-[3(ethoxycarbonyl)benzoyl]benzenepropanoic acid ethyl ester

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Technology Process of 2-{[6-(4-Acetylphenyl)hexyl]oxy}-5-[3(ethoxycarbonyl)benzoyl]benzenepropanoic acid ethyl ester

There total 12 articles about 2-{[6-(4-Acetylphenyl)hexyl]oxy}-5-[3(ethoxycarbonyl)benzoyl]benzenepropanoic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 16424-56-9
trans 6-phenyl-5-hexenoic acid

: 128577-90-2
2-{[6-(4-Acetylphenyl)hexyl]oxy}-5-[3(ethoxycarbonyl)benzoyl]benzenepropanoic acid ethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 95 percent / H₂ / 5percent Pd/C / ethyl acetate / 1 h / 25 °C / 1551.4 Torr

2: 91 percent / LiAlH₄ / diethyl ether / 4 h / 25 °C

3: 43 percent / AlCl₃ / CH₂Cl₂ / 25 °C

4: triethylamine (TEA) / diethyl ether

5: 1.) 60percent sodium hydride disp. in oil / 1.) DMF, 25 deg C, 30 min, 2.) 65 deg C

With lithium aluminium tetrahydride; aluminium trichloride; hydrogen; sodium hydride; triethylamine; palladium on activated charcoal; In diethyl ether; dichloromethane; ethyl acetate;
DOI:10.1021/jm00172a020

Reference yield:

: 17814-85-6
(4-carboxybutyl)triphenylphosphonium bromide

: 128577-90-2
2-{[6-(4-Acetylphenyl)hexyl]oxy}-5-[3(ethoxycarbonyl)benzoyl]benzenepropanoic acid ethyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) lithium hexamethyldisilazide / 1.) THF, hexane, 25 deg C, 1 h, 2.) 25 deg C, 2 h

2: 95 percent / H₂ / 5percent Pd/C / ethyl acetate / 1 h / 25 °C / 1551.4 Torr

3: 91 percent / LiAlH₄ / diethyl ether / 4 h / 25 °C

4: 43 percent / AlCl₃ / CH₂Cl₂ / 25 °C

5: triethylamine (TEA) / diethyl ether

6: 1.) 60percent sodium hydride disp. in oil / 1.) DMF, 25 deg C, 30 min, 2.) 65 deg C

With lithium aluminium tetrahydride; aluminium trichloride; hydrogen; sodium hydride; triethylamine; lithium hexamethyldisilazane; palladium on activated charcoal; In diethyl ether; dichloromethane; ethyl acetate;
DOI:10.1021/jm00172a020

Reference yield:

: 100-52-7
benzaldehyde

: 128577-90-2
2-{[6-(4-Acetylphenyl)hexyl]oxy}-5-[3(ethoxycarbonyl)benzoyl]benzenepropanoic acid ethyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) lithium hexamethyldisilazide / 1.) THF, hexane, 25 deg C, 1 h, 2.) 25 deg C, 2 h

2: 95 percent / H₂ / 5percent Pd/C / ethyl acetate / 1 h / 25 °C / 1551.4 Torr

3: 91 percent / LiAlH₄ / diethyl ether / 4 h / 25 °C

4: 43 percent / AlCl₃ / CH₂Cl₂ / 25 °C

5: triethylamine (TEA) / diethyl ether

6: 1.) 60percent sodium hydride disp. in oil / 1.) DMF, 25 deg C, 30 min, 2.) 65 deg C

With lithium aluminium tetrahydride; aluminium trichloride; hydrogen; sodium hydride; triethylamine; lithium hexamethyldisilazane; palladium on activated charcoal; In diethyl ether; dichloromethane; ethyl acetate;
DOI:10.1021/jm00172a020