5-phenyl-2,4-hexadienal

Base Information

• Chemical Name: 5-phenyl-2,4-hexadienal
• CAS No.: 91962-53-7
• Molecular Formula: C₁₂H₁₂O
• Molecular Weight: 172.227
• Mol file: 91962-53-7.mol

Synonyms:5-phenyl-2,4-hexadienal

Chemical Property of 5-phenyl-2,4-hexadienal

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of 5-phenyl-2,4-hexadienal

There total 3 articles about 5-phenyl-2,4-hexadienal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

(E)-(4-Oxo-2-butenyl)phosphonsaeure-diethylester (110905-37-8) + acetophenone (98-86-2) → 5-phenyl-2,4-hexadienal (91962-53-7)

Guidance literature:

With cyclohexylamine; lithium diisopropyl amide; In tetrahydrofuran; at 0 - 25 ℃; for 111h;

DOI:10.1021/jo00306a006

Reference yield:

3-(N-Methylanilino)-2-propenal (14189-82-3) → 5-phenyl-2,4-hexadienal (91962-53-7)

Guidance literature:

In diethyl ether; benzene;

Reference yield:

N-methylaniline (100-61-8) → 5-phenyl-2,4-hexadienal (91962-53-7)

Guidance literature:

Multi-step reaction with 2 steps

1: benzene

2: benzene; diethyl ether

In diethyl ether; benzene;

upstream raw materials:

(E)-(4-Oxo-2-butenyl)phosphonsaeure-diethylester

acetophenone

3-(N-Methylanilino)-2-propenal

N-methylaniline

Refernces