(S,S)-N,N'-bis(5H-dibenzo[a,d]cyclohepten-5-yl)-1,2-diphenyl-1,2-ethylenediamine

Base Information

Chemical Name:(S,S)-N,N'-bis(5H-dibenzo[a,d]cyclohepten-5-yl)-1,2-diphenyl-1,2-ethylenediamine
CAS No.:858370-95-3
Molecular Formula:C₄₄H₃₆N₂
Molecular Weight:592.783
Hs Code.:

Synonyms:(S,S)-N,N'-bis(5H-dibenzo[a,d]cyclohepten-5-yl)-1,2-diphenyl-1,2-ethylenediamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S,S)-N,N'-bis(5H-dibenzo[a,d]cyclohepten-5-yl)-1,2-diphenyl-1,2-ethylenediamine

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Technology Process of (S,S)-N,N'-bis(5H-dibenzo[a,d]cyclohepten-5-yl)-1,2-diphenyl-1,2-ethylenediamine

There total 1 articles about (S,S)-N,N'-bis(5H-dibenzo[a,d]cyclohepten-5-yl)-1,2-diphenyl-1,2-ethylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 29841-69-8
(S,S)-1,2-diphenyl-1,2-diaminoethane

: 18506-04-2
5-chloro-5H-dibenzo[a,d]cycloheptene

: 858370-95-3
(S,S)-N,N'-bis(5H-dibenzo[a,d]cyclohepten-5-yl)-1,2-diphenyl-1,2-ethylenediamine

Guidance literature:: With triethylamine; In dichloromethane; for 0.166667h; Heating;
DOI:10.1002/anie.200502036

Reference yield: 93.0%

: 858370-95-3
(S,S)-N,N'-bis(5H-dibenzo[a,d]cyclohepten-5-yl)-1,2-diphenyl-1,2-ethylenediamine

: bis(1,5-cyclooctadiene)rhodium(I) trifluoromethanesulfonate

: 75-09-2
dichloromethane

: [Rh((S,S)-N,N'-bis(5H-dibenzo[a,d]cyclohepten-5-yl)-1,2-diphenyl-1,2-ethylenediamine)](O₃SCF₃)*CH₂Cl₂

Guidance literature:: In dichloromethane; (Ar); glovebox; soln. of ligand (1 equiv.) and Rh complex in CH2Cl2 was stirred at room temp. for 1 h; layered with hexane overnight; decanted; dried (vac.);
DOI:10.1021/om0500927