cis-2-(3,4-dimethoxyphenyl)-6,7-methylenedioxy-1-(N-methylformamido)-1,2,3,4-tetrahydronaphthalene

Base Information

Chemical Name:cis-2-(3,4-dimethoxyphenyl)-6,7-methylenedioxy-1-(N-methylformamido)-1,2,3,4-tetrahydronaphthalene
CAS No.:105594-85-2
Molecular Formula:C₂₁H₂₃NO₅
Molecular Weight:369.417
Hs Code.:

Synonyms:cis-2-(3,4-dimethoxyphenyl)-6,7-methylenedioxy-1-(N-methylformamido)-1,2,3,4-tetrahydronaphthalene

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Chemical Property of cis-2-(3,4-dimethoxyphenyl)-6,7-methylenedioxy-1-(N-methylformamido)-1,2,3,4-tetrahydronaphthalene

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Technology Process of cis-2-(3,4-dimethoxyphenyl)-6,7-methylenedioxy-1-(N-methylformamido)-1,2,3,4-tetrahydronaphthalene

There total 2 articles about cis-2-(3,4-dimethoxyphenyl)-6,7-methylenedioxy-1-(N-methylformamido)-1,2,3,4-tetrahydronaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.3%

: 75-87-6
chloral

: 105594-81-8
cis-2-(3,4-dimethoxyphenyl)-N-methyl-6,7-methylenedioxy-1,2,3,4-tetrahydro-1-naphthylamine

: 105594-85-2
cis-2-(3,4-dimethoxyphenyl)-6,7-methylenedioxy-1-(N-methylformamido)-1,2,3,4-tetrahydronaphthalene

Guidance literature:: In chloroform; for 2h; Heating;
DOI:10.1248/cpb.33.4139

Reference yield:

: 41303-46-2
2-(3,4-dimethoxyphenyl)-6,7-methylenedioxy-3,4-dihydronaphthalen-1(2H)-one

: 105594-85-2
cis-2-(3,4-dimethoxyphenyl)-6,7-methylenedioxy-1-(N-methylformamido)-1,2,3,4-tetrahydronaphthalene

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) titanium tetrachloride; 2.) sodium borohydride / 1.) CHCl₃, reflux, 0.5 h; 2.) methanol, 1 h, r.t.

2: 87.3 percent / CHCl₃ / 2 h / Heating

With sodium tetrahydroborate; titanium tetrachloride; In chloroform;
DOI:10.1248/cpb.33.4139