(3R,4S)-4--3-(methoxymethoxy)-5-phenylpent-1-ene

Base Information

Chemical Name:(3R,4S)-4--3-(methoxymethoxy)-5-phenylpent-1-ene
CAS No.:229981-23-1
Molecular Formula:C₁₉H₂₉NO₄
Molecular Weight:335.444
Hs Code.:

(3R,4S)-4-<N-(tert-butoxycarbonyl)-N-methylamino>-3-(methoxymethoxy)-5-phenylpent-1-ene

Synonyms:(3R,4S)-4--3-(methoxymethoxy)-5-phenylpent-1-ene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3R,4S)-4--3-(methoxymethoxy)-5-phenylpent-1-ene

Chemical Property:

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Technology Process of (3R,4S)-4--3-(methoxymethoxy)-5-phenylpent-1-ene

There total 4 articles about (3R,4S)-4--3-(methoxymethoxy)-5-phenylpent-1-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 229981-21-9
(3R,4S)-N-(tert-butoxycarbonyl)-4-amino-3-(methoxymethoxy)-5-phenylpent-1-ene

: 74-88-4
methyl iodide

: 229981-23-1
(3R,4S)-4--3-(methoxymethoxy)-5-phenylpent-1-ene

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; for 15h; Ambient temperature;
DOI:10.1021/jo990200x

Reference yield:

: 124915-64-6
(4S,5R)-5-ethenyl-4-phenylmethyloxazolidin-2-one

: 229981-23-1
(3R,4S)-4--3-(methoxymethoxy)-5-phenylpent-1-ene

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / Et₃N, DMAP / tetrahydrofuran / 5.5 h / Ambient temperature

2: 76 percent / Cs₂CO₃ / methanol / 25 h / Ambient temperature

3: 95 percent / i-Pr₂NEt / CH₂Cl₂ / 1.) 0 deg C, 1 h, 2.) room temperature, 8 h

4: 96 percent / NaH / dimethylformamide / 15 h / Ambient temperature

With dmap; sodium hydride; caesium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo990200x

Reference yield:

: 99113-30-1
((1S,2R)-1-benzyl-2-hydroxybut-3-enyl)carbamic acid tert-butyl ester

: 229981-23-1
(3R,4S)-4--3-(methoxymethoxy)-5-phenylpent-1-ene

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / i-Pr₂NEt / CH₂Cl₂ / 1.) 0 deg C, 1 h, 2.) room temperature, 8 h

2: 96 percent / NaH / dimethylformamide / 15 h / Ambient temperature

With sodium hydride; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo990200x