((5-(benzyloxy)-2-methylenepent-3-yn-1-yl)oxy)(tert-butyl)dimethylsilane

Base Information

Chemical Name:((5-(benzyloxy)-2-methylenepent-3-yn-1-yl)oxy)(tert-butyl)dimethylsilane
CAS No.:1373264-21-1
Molecular Formula:C₁₉H₂₈O₂Si
Molecular Weight:316.516
Hs Code.:

Synonyms:((5-(benzyloxy)-2-methylenepent-3-yn-1-yl)oxy)(tert-butyl)dimethylsilane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ((5-(benzyloxy)-2-methylenepent-3-yn-1-yl)oxy)(tert-butyl)dimethylsilane

Chemical Property:

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Technology Process of ((5-(benzyloxy)-2-methylenepent-3-yn-1-yl)oxy)(tert-butyl)dimethylsilane

There total 1 articles about ((5-(benzyloxy)-2-methylenepent-3-yn-1-yl)oxy)(tert-butyl)dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 4039-82-1
Benzyl propargyl ether

: 147455-22-9
1-(tert-butyldimethylsilyloxy)-2-iodoprop-2-ene

: 1373264-21-1
((5-(benzyloxy)-2-methylenepent-3-yn-1-yl)oxy)(tert-butyl)dimethylsilane

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diisopropylamine; In tetrahydrofuran; at 50 ℃; Inert atmosphere;
DOI:10.1021/jo300294r

Reference yield: 34.0%

: 1373264-21-1
((5-(benzyloxy)-2-methylenepent-3-yn-1-yl)oxy)(tert-butyl)dimethylsilane

: 55962-05-5
[N-(p-tolylsulfonyl)imino]phenyliodinane

: 1373263-74-1
2-(3-(benzyloxy)prop-1-yn-1-yl)-2-(((tert-butyldimethylsilyl)oxy)-methyl)-1-tosylaziridine

Guidance literature:: With tetrakis(acetonitrile)copper(I) perchlorate; In acetonitrile; at 20 ℃; Molecular sieve; Ionic liquid;
DOI:10.1021/jo300294r

Reference yield:

: 1373264-21-1
((5-(benzyloxy)-2-methylenepent-3-yn-1-yl)oxy)(tert-butyl)dimethylsilane

: 1373265-25-8
4'-(((tert-butyldimethylsilyl)oxy)methyl)-1'-tosyl-1',5'-dihydrospiro[isochroman-4,2'-pyrrole]

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(acetonitrile)copper(I) perchlorate / acetonitrile / 20 °C / Molecular sieve; Ionic liquid

2: Echavarren catalyst / dichloromethane / 1 h / 0 - 20 °C

With tetrakis(acetonitrile)copper(I) perchlorate; Echavarren catalyst; In dichloromethane; acetonitrile;
DOI:10.1021/jo300294r