ethyl 10-benzyl-9,11-dioxo-6,9,10,11-tetrahydro-5H-pyrrolo-[3′,4′:3,4]pyrrolo[2,1-a]isoquinoline-8-carboxylate

Base Information

• Chemical Name: ethyl 10-benzyl-9,11-dioxo-6,9,10,11-tetrahydro-5H-pyrrolo-[3′,4′:3,4]pyrrolo[2,1-a]isoquinoline-8-carboxylate
• CAS No.: 1264932-17-3
• Molecular Formula: C₂₄H₂₀N₂O₄
• Molecular Weight: 400.434

Synonyms:ethyl 10-benzyl-9,11-dioxo-6,9,10,11-tetrahydro-5H-pyrrolo-[3′,4′:3,4]pyrrolo[2,1-a]isoquinoline-8-carboxylate

Chemical Property of ethyl 10-benzyl-9,11-dioxo-6,9,10,11-tetrahydro-5H-pyrrolo-[3′,4′:3,4]pyrrolo[2,1-a]isoquinoline-8-carboxylate

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Technology Process of ethyl 10-benzyl-9,11-dioxo-6,9,10,11-tetrahydro-5H-pyrrolo-[3′,4′:3,4]pyrrolo[2,1-a]isoquinoline-8-carboxylate

There total 4 articles about ethyl 10-benzyl-9,11-dioxo-6,9,10,11-tetrahydro-5H-pyrrolo-[3′,4′:3,4]pyrrolo[2,1-a]isoquinoline-8-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

1-benzyl-1H-pyrrole-2,5-dione (1631-26-1) + (3,4-dihydro-1H-isoquinolin-2-yl)-acetic acid ethyl ester (88014-09-9) → ethyl 10-benzyl-9,11-dioxo-6,9,10,11-tetrahydro-5H-pyrrolo-[3′,4′:3,4]pyrrolo[2,1-a]isoquinoline-8-carboxylate (1264932-17-3)

Guidance literature:

With tert.-butylhydroperoxide; potassium iodide; In water; N,N-dimethyl-formamide; at 80 ℃; for 9h; Green chemistry;

DOI:10.1039/c4ra03455d

Reference yield: 78.0%

→ ethyl 10-benzyl-9,11-dioxo-6,9,10,11-tetrahydro-5H-pyrrolo-[3′,4′:3,4]pyrrolo[2,1-a]isoquinoline-8-carboxylate (1264932-17-3)

Guidance literature:

With oxygen; copper(I) bromide; In acetonitrile; at 60 ℃; for 10h;

Reference yield: 68.0%

1-(phenylmethyl)-2,5-pyrrolidinedione (2142-06-5) + (3,4-dihydro-1H-isoquinolin-2-yl)-acetic acid ethyl ester (88014-09-9) → ethyl 10-benzyl-9,11-dioxo-6,9,10,11-tetrahydro-5H-pyrrolo-[3′,4′:3,4]pyrrolo[2,1-a]isoquinoline-8-carboxylate (1264932-17-3)

Guidance literature:

With N-Bromosuccinimide; In acetonitrile; at 20 ℃; for 2h; UV-irradiation;

DOI:10.1039/c3cc44486d

upstream raw materials:

1-benzyl-1H-pyrrole-2,5-dione

(3,4-dihydro-1H-isoquinolin-2-yl)-acetic acid ethyl ester

1-(phenylmethyl)-2,5-pyrrolidinedione

1,2,3,4-tetrahydroisoquinoline

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