isopropyl 2-(4-chlorophenyl)-2-oxoacetate

Base Information

Chemical Name:isopropyl 2-(4-chlorophenyl)-2-oxoacetate
CAS No.:30565-44-7
Molecular Formula:C₁₁H₁₁ClO₃
Molecular Weight:226.66
Hs Code.:

Synonyms:isopropyl 2-(4-chlorophenyl)-2-oxoacetate

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Chemical Property of isopropyl 2-(4-chlorophenyl)-2-oxoacetate

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Technology Process of isopropyl 2-(4-chlorophenyl)-2-oxoacetate

There total 7 articles about isopropyl 2-(4-chlorophenyl)-2-oxoacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 103807-49-4
Bromo-(4-chloro-phenyl)-acetic acid isopropyl ester

: 30565-44-7
isopropyl 2-(4-chlorophenyl)-2-oxoacetate

Guidance literature:: With 4-methoxypyridine; tris(2,2'-bipyridine)ruthenium dichloride; lithium carbonate; In N,N-dimethyl acetamide; at 25 ℃; for 24h; Irradiation;
DOI:10.1021/ol2002013

Reference yield:

: 34966-48-8
ethyl 2-(4-chlorophenyl)-2-oxoacetate

: 30565-44-7
isopropyl 2-(4-chlorophenyl)-2-oxoacetate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / Inert atmosphere

2: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 20 °C / Inert atmosphere

3: triethylamine / dichloromethane / 20 °C / Inert atmosphere

With oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; sodium hydroxide; In dichloromethane;
DOI:10.1039/c4cc00427b

Reference yield:

: 637-87-6
1-Chloro-4-iodobenzene

: 201230-82-2
carbon monoxide

: 67-63-0,8013-70-5
isopropyl alcohol

: 22913-11-7
isopropyl 4-chlorobenzoate

: 30565-44-7
isopropyl 2-(4-chlorophenyl)-2-oxoacetate

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; triethylamine; at 80 ℃; for 12h; under 114000 Torr;
DOI:10.1021/jo00235a017