2'-(9H-fluoren-9-yl)methoxycarbonylaminoethyl 4-O-[3-O-acetyl-4-O-benzyl-2-deoxy-6-O-(tert-butyldiphenylsilyl)-2-(trichloroethylcarbonylamino)-β-D-glucopyranosyl]-2,3,6-tri-O-benzyl-β-D-glucopyranoside

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Chemical Name:2'-(9H-fluoren-9-yl)methoxycarbonylaminoethyl 4-O-[3-O-acetyl-4-O-benzyl-2-deoxy-6-O-(tert-butyldiphenylsilyl)-2-(trichloroethylcarbonylamino)-β-D-glucopyranosyl]-2,3,6-tri-O-benzyl-β-D-glucopyranoside
CAS No.:1386972-56-0
Molecular Formula:C₇₈H₈₃Cl₃N₂O₁₅Si
Molecular Weight:1422.97
Hs Code.:

2'-(9H-fluoren-9-yl)methoxycarbonylaminoethyl 4-O-[3-O-acetyl-4-O-benzyl-2-deoxy-6-O-(tert-butyldiphenylsilyl)-2-(trichloroethylcarbonylamino)-β-D-glucopyranosyl]-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Synonyms:2'-(9H-fluoren-9-yl)methoxycarbonylaminoethyl 4-O-[3-O-acetyl-4-O-benzyl-2-deoxy-6-O-(tert-butyldiphenylsilyl)-2-(trichloroethylcarbonylamino)-β-D-glucopyranosyl]-2,3,6-tri-O-benzyl-β-D-glucopyranoside

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Chemical Property of 2'-(9H-fluoren-9-yl)methoxycarbonylaminoethyl 4-O-[3-O-acetyl-4-O-benzyl-2-deoxy-6-O-(tert-butyldiphenylsilyl)-2-(trichloroethylcarbonylamino)-β-D-glucopyranosyl]-2,3,6-tri-O-benzyl-β-D-glucopyranoside

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Technology Process of 2'-(9H-fluoren-9-yl)methoxycarbonylaminoethyl 4-O-[3-O-acetyl-4-O-benzyl-2-deoxy-6-O-(tert-butyldiphenylsilyl)-2-(trichloroethylcarbonylamino)-β-D-glucopyranosyl]-2,3,6-tri-O-benzyl-β-D-glucopyranoside

There total 1 articles about 2'-(9H-fluoren-9-yl)methoxycarbonylaminoethyl 4-O-[3-O-acetyl-4-O-benzyl-2-deoxy-6-O-(tert-butyldiphenylsilyl)-2-(trichloroethylcarbonylamino)-β-D-glucopyranosyl]-2,3,6-tri-O-benzyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1386972-65-1
2'-(9H-fluoren-9-yl)methoxycarbonylaminoethyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside

: 1386972-53-7
thiotolyl 3-O-acetyl-4-O-benzyl-6-O-(tert-butyldiphenylsilyl)-2-deoxy-2-(trichloroethylcarbonylamino)-β-D-glucopyranoside

: 1386972-56-0
2'-(9H-fluoren-9-yl)methoxycarbonylaminoethyl 4-O-[3-O-acetyl-4-O-benzyl-2-deoxy-6-O-(tert-butyldiphenylsilyl)-2-(trichloroethylcarbonylamino)-β-D-glucopyranosyl]-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: 2'-(9H-fluoren-9-yl)methoxycarbonylaminoethyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside; thiotolyl 3-O-acetyl-4-O-benzyl-6-O-(tert-butyldiphenylsilyl)-2-deoxy-2-(trichloroethylcarbonylamino)-β-D-glucopyranoside; In diethyl ether; 1,2-dichloro-ethane; toluene; at 20 ℃; for 2h; Molecular sieve;

With N-iodo-succinimide; trifluorormethanesulfonic acid; In diethyl ether; 1,2-dichloro-ethane; toluene; at -30 ℃; for 6h; Molecular sieve;
DOI:10.1080/07328303.2012.658274

Reference yield: 91.0%

: 1386972-56-0
2'-(9H-fluoren-9-yl)methoxycarbonylaminoethyl 4-O-[3-O-acetyl-4-O-benzyl-2-deoxy-6-O-(tert-butyldiphenylsilyl)-2-(trichloroethylcarbonylamino)-β-D-glucopyranosyl]-2,3,6-tri-O-benzyl-β-D-glucopyranoside

: 1386972-58-2
2'-(9H-fluoren-9-yl)methoxycarbonylaminoethyl 4-O-[3-O-acetyl-2-azido-4-O-benzyl-2-deoxy-6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranosyl]-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: 2'-(9H-fluoren-9-yl)methoxycarbonylaminoethyl 4-O-[3-O-acetyl-4-O-benzyl-2-deoxy-6-O-(tert-butyldiphenylsilyl)-2-(trichloroethylcarbonylamino)-β-D-glucopyranosyl]-2,3,6-tri-O-benzyl-β-D-glucopyranoside; With indium; ammonium chloride; In ethanol; water; at 98 ℃; for 6h;

With triflic azide; potassium carbonate; copper(II) sulfate; In methanol; dichloromethane; water; at 0 - 20 ℃; for 10h;
DOI:10.1080/07328303.2012.658274