4-methoxy-N-(4-methoxyphenyl)-N-{4-[2-(trimethylsilyl)ethynyl]phenyl}aniline

Base Information

Chemical Name:4-methoxy-N-(4-methoxyphenyl)-N-{4-[2-(trimethylsilyl)ethynyl]phenyl}aniline
CAS No.:218608-72-1
Molecular Formula:C₂₅H₂₇NO₂Si
Molecular Weight:401.58
Hs Code.:

Synonyms:4-methoxy-N-(4-methoxyphenyl)-N-{4-[2-(trimethylsilyl)ethynyl]phenyl}aniline

Suppliers and Price of 4-methoxy-N-(4-methoxyphenyl)-N-{4-[2-(trimethylsilyl)ethynyl]phenyl}aniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 4-methoxy-N-(4-methoxyphenyl)-N-{4-[2-(trimethylsilyl)ethynyl]phenyl}aniline

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of 4-methoxy-N-(4-methoxyphenyl)-N-{4-[2-(trimethylsilyl)ethynyl]phenyl}aniline

There total 13 articles about 4-methoxy-N-(4-methoxyphenyl)-N-{4-[2-(trimethylsilyl)ethynyl]phenyl}aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.3%

: 201802-15-5
N,N-bis(4-methoxyphenyl)-4'-iodophenylamine

: 1066-54-2
trimethylsilylacetylene

: 218608-72-1
4-methoxy-N-(4-methoxyphenyl)-N-{4-[2-(trimethylsilyl)ethynyl]phenyl}aniline

Guidance literature:: With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; diisopropylamine; In toluene; at 70 ℃; for 13h; Inert atmosphere;

Reference yield: 90.0%

: 194416-45-0
4-bromo-N,N-bis-(4-methoxyphenyl)aniline

: 1066-54-2
trimethylsilylacetylene

: 218608-72-1
4-methoxy-N-(4-methoxyphenyl)-N-{4-[2-(trimethylsilyl)ethynyl]phenyl}aniline

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) iodide; triethylamine; potassium iodide; In tetrahydrofuran; at 90 ℃; for 60h; Schlenk technique; Darkness;
DOI:10.1055/s-0034-1378818

Reference yield: 75.0%

: 101-70-2
bis(4-methoxyphenyl)amine

: 16116-78-2
(4-bromophenyl)(trimethylsilyl)acetylene

: 218608-72-1
4-methoxy-N-(4-methoxyphenyl)-N-{4-[2-(trimethylsilyl)ethynyl]phenyl}aniline

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri-tert-butyl phosphine; sodium t-butanolate; In hexane; toluene; at 80 ℃; for 12h; Inert atmosphere;
DOI:10.1039/c1jm10993f