Diazenecarboxylic acid, (4-methylphenyl)-, 1,1-dimethylethyl ester (9CI)

Base Information

Chemical Name:Diazenecarboxylic acid, (4-methylphenyl)-, 1,1-dimethylethyl ester (9CI)
CAS No.:773893-07-5
Molecular Formula:C12H16 N2 O2
Molecular Weight:220.271
Hs Code.:
Mol file:773893-07-5.mol

Synonyms:Diazenecarboxylic acid, (4-methylphenyl)-, 1,1-dimethylethyl ester (9CI)

Suppliers and Price of Diazenecarboxylic acid, (4-methylphenyl)-, 1,1-dimethylethyl ester (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of Diazenecarboxylic acid, (4-methylphenyl)-, 1,1-dimethylethyl ester (9CI)

Chemical Property:

PSA：51.02000
LogP:4.01380

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Diazenecarboxylic acid, (4-methylphenyl)-, 1,1-dimethylethyl ester (9CI)

There total 5 articles about Diazenecarboxylic acid, (4-methylphenyl)-, 1,1-dimethylethyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 93138-89-7
tert-butyl 2-(p-tolyl)hydrazine-1-carboxylate

: 773893-07-5
tert-butyl 2-(4-methylphenyl)azocarboxylate

Guidance literature:: With manganese(IV) oxide; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1021/acs.orglett.8b00448

Reference yield: 91.0%

: 870-46-2
t-butoxycarbonylhydrazine

: 107536-32-3
tris(4-methylphenyl)bismuth diacetate

: 773893-07-5
tert-butyl 2-(4-methylphenyl)azocarboxylate

: 93138-89-7
tert-butyl 2-(p-tolyl)hydrazine-1-carboxylate

Guidance literature:: With copper diacetate; 2,5-tert-butyl-4-methyl-phenol; In dichloromethane; at -60 ℃; Further Variations:; Temperatures; Product distribution;
DOI:10.1016/j.tet.2004.07.020

Reference yield:

: 539-44-6
N-4-methylphenylhydrazine

: 773893-07-5
tert-butyl 2-(4-methylphenyl)azocarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 4 h / 20 °C

2: manganese(IV) oxide / dichloromethane / 1 h / 20 °C

With manganese(IV) oxide; triethylamine; In dichloromethane;
DOI:10.1021/acs.orglett.8b00448