3-<4-<(tert-Butyldimethylsilyl)oxy>-2,3,5-trimethylphenoxy>propyl bromide

Base Information

Chemical Name:3-<4-<(tert-Butyldimethylsilyl)oxy>-2,3,5-trimethylphenoxy>propyl bromide
CAS No.:112109-68-9
Molecular Formula:C₁₈H₃₁BrO₂Si
Molecular Weight:387.432
Hs Code.:

Synonyms:3-<4-<(tert-Butyldimethylsilyl)oxy>-2,3,5-trimethylphenoxy>propyl bromide

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Chemical Property of 3-<4-<(tert-Butyldimethylsilyl)oxy>-2,3,5-trimethylphenoxy>propyl bromide

Chemical Property:

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Technology Process of 3-<4-<(tert-Butyldimethylsilyl)oxy>-2,3,5-trimethylphenoxy>propyl bromide

There total 4 articles about 3-<4-<(tert-Butyldimethylsilyl)oxy>-2,3,5-trimethylphenoxy>propyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 109-64-8
1,3-dibromo-propane

: 112136-00-2
4-(tert-butyldimethylsilyloxy)-2,3,5-trimethylphenol

: 112109-68-9
3-<4-<(tert-Butyldimethylsilyl)oxy>-2,3,5-trimethylphenoxy>propyl bromide

Guidance literature:: With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; sodium carbonate; In water; for 2h; Ambient temperature;
DOI:10.1021/jm00122a022

Reference yield:

: 700-13-0
Trimethylhydroquinone

: 112109-68-9
3-<4-<(tert-Butyldimethylsilyl)oxy>-2,3,5-trimethylphenoxy>propyl bromide

Guidance literature:: Multi-step reaction with 4 steps

1: 87 percent / pyridine / CH₂Cl₂ / Ambient temperature

2: 98 percent / imidazole / dimethylformamide / Ambient temperature

3: KOH / dimethylformamide; methanol / 48 h

4: 46 percent / Na₂CO₃, tetrabutylammonium hydrogen sulfate, NaOH / H₂O / 2 h / Ambient temperature

With pyridine; 1H-imidazole; potassium hydroxide; sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; sodium carbonate; In methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00122a022

Reference yield:

: 112109-69-0
4-hydroxy-2,3,5-trimethylphenyl pivalate

: 112109-68-9
3-<4-<(tert-Butyldimethylsilyl)oxy>-2,3,5-trimethylphenoxy>propyl bromide

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / imidazole / dimethylformamide / Ambient temperature

2: KOH / dimethylformamide; methanol / 48 h

3: 46 percent / Na₂CO₃, tetrabutylammonium hydrogen sulfate, NaOH / H₂O / 2 h / Ambient temperature

With 1H-imidazole; potassium hydroxide; sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; sodium carbonate; In methanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00122a022