E-1-[3-acetoxy-5-benzyloxyphenyl]-2-[4-benzyloxy-3-methoxyphenyl]-ethene

Base Information

Chemical Name:E-1-[3-acetoxy-5-benzyloxyphenyl]-2-[4-benzyloxy-3-methoxyphenyl]-ethene
CAS No.:1408062-09-8
Molecular Formula:C₃₁H₂₈O₅
Molecular Weight:480.56
Hs Code.:

Synonyms:E-1-[3-acetoxy-5-benzyloxyphenyl]-2-[4-benzyloxy-3-methoxyphenyl]-ethene

Suppliers and Price of E-1-[3-acetoxy-5-benzyloxyphenyl]-2-[4-benzyloxy-3-methoxyphenyl]-ethene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of E-1-[3-acetoxy-5-benzyloxyphenyl]-2-[4-benzyloxy-3-methoxyphenyl]-ethene

Chemical Property:

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Technology Process of E-1-[3-acetoxy-5-benzyloxyphenyl]-2-[4-benzyloxy-3-methoxyphenyl]-ethene

There total 9 articles about E-1-[3-acetoxy-5-benzyloxyphenyl]-2-[4-benzyloxy-3-methoxyphenyl]-ethene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 1408062-10-1
3-acetoxy-5-benzyloxybenzoyl chloride

: 55708-65-1
1-(benzyloxy)-4-ethenyl-2-methoxybenzene

: 1408062-09-8
E-1-[3-acetoxy-5-benzyloxyphenyl]-2-[4-benzyloxy-3-methoxyphenyl]-ethene

Guidance literature:: With N-ethylmorpholine;; palladium diacetate; 1,3-bis[2,6-diisopropylphenyl]imidazolium chloride; In 5,5-dimethyl-1,3-cyclohexadiene; at 130 ℃; Inert atmosphere; Reflux;
DOI:10.1016/j.ejmech.2013.02.017

Reference yield:

: 100-39-0
benzyl bromide

: 1408062-09-8
E-1-[3-acetoxy-5-benzyloxyphenyl]-2-[4-benzyloxy-3-methoxyphenyl]-ethene

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 4 h / 0 - 20 °C / Inert atmosphere

2.1: potassium tert-butylate / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

2.2: 2 h

3.1: palladium diacetate; N-ethylmorpholine; / xylene / 130 °C / Inert atmosphere

With potassium tert-butylate; sodium hydride; N-ethylmorpholine;; palladium diacetate; In tetrahydrofuran; N,N-dimethyl-formamide; xylene; mineral oil;

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 1408062-09-8
E-1-[3-acetoxy-5-benzyloxyphenyl]-2-[4-benzyloxy-3-methoxyphenyl]-ethene

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 4 h / 0 - 20 °C / Inert atmosphere

2.1: potassium tert-butylate / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

2.2: 2 h

3.1: palladium diacetate; N-ethylmorpholine; / xylene / 130 °C / Inert atmosphere

With potassium tert-butylate; sodium hydride; N-ethylmorpholine;; palladium diacetate; In tetrahydrofuran; N,N-dimethyl-formamide; xylene; mineral oil;