2-bromo-6-[4-(4-methylpiperazin-1-yl)phenyl]-4-(2-trimethylsilanylethoxymethyl)-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene

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Chemical Name:2-bromo-6-[4-(4-methylpiperazin-1-yl)phenyl]-4-(2-trimethylsilanylethoxymethyl)-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene
CAS No.:1469858-69-2
Molecular Formula:C₂₅H₃₃BrN₄OSSi
Molecular Weight:545.619
Hs Code.:

Synonyms:2-bromo-6-[4-(4-methylpiperazin-1-yl)phenyl]-4-(2-trimethylsilanylethoxymethyl)-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene

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Chemical Property of 2-bromo-6-[4-(4-methylpiperazin-1-yl)phenyl]-4-(2-trimethylsilanylethoxymethyl)-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene

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Technology Process of 2-bromo-6-[4-(4-methylpiperazin-1-yl)phenyl]-4-(2-trimethylsilanylethoxymethyl)-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene

There total 6 articles about 2-bromo-6-[4-(4-methylpiperazin-1-yl)phenyl]-4-(2-trimethylsilanylethoxymethyl)-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1469858-59-0
6-[4-(4-methylpiperazin-1-yl)phenyl]-4-(2-trimethylsilanylethoxymethyl)-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene

: 1469858-69-2
2-bromo-6-[4-(4-methylpiperazin-1-yl)phenyl]-4-(2-trimethylsilanylethoxymethyl)-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene

Guidance literature:: With N-Bromosuccinimide; In dichloromethane; for 2h;

Reference yield:

: 1469857-12-2
6-(4-bromophenyl)-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene

: 1469858-69-2
2-bromo-6-[4-(4-methylpiperazin-1-yl)phenyl]-4-(2-trimethylsilanylethoxymethyl)-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / tetrahydrofuran; mineral oil / 0 - 80 °C

2: caesium carbonate; palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / 1,4-dioxane / 8 h / 100 °C

3: N-Bromosuccinimide / dichloromethane / 2 h

With N-Bromosuccinimide; palladium diacetate; sodium hydride; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In tetrahydrofuran; 1,4-dioxane; dichloromethane; mineral oil;

Reference yield:

: 1469858-10-3
6-(4-bromophenyl)-4-(2-trimethylsilanylethoxymethyl)-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene

: 1469858-69-2
2-bromo-6-[4-(4-methylpiperazin-1-yl)phenyl]-4-(2-trimethylsilanylethoxymethyl)-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate; palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / 1,4-dioxane / 8 h / 100 °C

2: N-Bromosuccinimide / dichloromethane / 2 h

With N-Bromosuccinimide; palladium diacetate; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,4-dioxane; dichloromethane;